Preparation method of high stability high frequency wide temperature magnetic core material used for numerical control magnetic core pendulum feeder
A high-stability, magnetic core material technology, applied in the field of preparation of high-stability, high-frequency, wide-temperature magnetic core materials for numerically controlled magnetic core swinging machines, can solve the problem that soft ferrite does not have stable use, and achieve excellent DC superposition characteristics, excellent overall performance, and the effect of high saturation magnetic flux density
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Embodiment 1
[0023] Accurately weigh 71.5mol of Fe 2 o 3 , 18.5mol of Mn 3 o 4 , 10mol of ZnO and corresponding mass parts of CaO, LaO, CuO, V 2 o 5 、TiO 2 、Co 2 o 3 , NiO, B 2 o 3 Standby, the composition included in the second component and the percentage of each component in the total mass of the first component are as follows: CaO 0.04%, LaO 0.023%, CuO 0.04%, V 2 o 5 0.08%, TiO 2 0.15%, Co 2 o 3 0.21%, NiO 0.3%, B 2 o 3 0.06%;
[0024] The weighed first component (Fe 2 o 3 , Mn 3 o 4 , ZnO) in a star-shaped ball mill for coarse grinding and mixing, then placed in an electric heating rotary kiln at 850°C for 3 hours, and after leaving the kiln, introduce it into a vibrating ball mill for vibration grinding for 20 minutes, and then add the weighed second group points (CaO, LaO, CuO, V 2 o 5 、TiO 2 、Co 2 o 3 , NiO, B 2 o 3 ) continue to grind and mix to obtain a powder mixture material with an average particle diameter of 1.0 μm, wherein the vibration frequ...
Embodiment 2
[0030] Accurately weigh 70mol of Fe 2 o 3 , 15mol of Mn 3 o 4 , 15mol of ZnO and corresponding mass parts of CaO, LaO, CuO, V 2 o 5 、TiO 2 、Co 2 o 3 , NiO, B 2 o 3 Standby, the components included in the second component and the percentages of each component in the total mass of the first component are as follows: CaO 0.02%, LaO 0.01%, CuO 0.03%, V 2 o 5 0.02%, TiO 2 0.05%, Co 2 o 3 0.2%, NiO 0.1%, B 2 o 3 0.05%;
[0031] The weighed first component (Fe 2 o 3 , Mn 3 o 4 , ZnO) in a star-shaped ball mill for coarse grinding and mixing, then placed in an electric heating rotary kiln at 900°C for pre-calcination for 2 hours, and after leaving the kiln, introduce it into a vibrating ball mill for vibration grinding for 30 minutes, and then add the weighed second group points (CaO, LaO, CuO, V 2 o 5 、TiO 2 、Co 2 o 3 , NiO, B 2 o 3 ) continue to grind and mix to obtain a powder mixture material with an average particle diameter of 0.8 μm, wherein the v...
Embodiment 3
[0037] The difference between embodiment 3 and embodiment 1 lies in the consumption of the first component and the second component, and other contents are exactly the same as embodiment 1.
[0038] The raw material in embodiment 3 is: the Fe of 72.5mol is accurately weighed 2 o 3 , 20mol of Mn 3 o 4 , 7.5mol of ZnO and corresponding mass parts of CaO, LaO, CuO, V 2 o 5 、TiO 2 、Co 2 o 3 , NiO, B 2 o 3 Standby, the ingredients included in the second component and the percentage of each ingredient in the total mass of the first component are as follows: CaO 0.06%, LaO 0.03%, CuO 0.05%, V 2 o 5 0.12%, TiO 2 0.18%, Co 2 o 3 0.22%, NiO 0.4%, B 2 o 3 0.08%.
[0039] Carry out performance test to the sample piece that above-mentioned method prepares, the result is as follows:
[0040] Density 4.97g / cm 3 , the initial permeability is 3730mT, the Curie temperature is 280°C, the saturation flux density at 500KHz, -40°C is 400mT, and the power loss is 85 kw / m 3 , a...
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