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Homogenization treatment and subsequent processing method suitable for magnesium alloy ingots

A technology of homogenization treatment and magnesium alloys, applied in the field of industrial magnesium alloys, can solve the problems of limited scope of action, increased alloy costs, improper element addition methods, etc., to improve comprehensive mechanical properties, reduce deformation residual stress, and reduce failure. effect of probability

Active Publication Date: 2014-05-21
GRIMAT ENG INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There are many ways to control the grain size of the alloy. For example, Zr element is often added to the rare earth magnesium alloy. Because it has a crystal structure and lattice constant similar to Mg, it can be used as a heterogeneous core to refine the grain size of the magnesium alloy. It is considered the most It is an effective refiner for refining the structure of magnesium alloys. In addition, it can also add alkaline earth elements and rare earth elements to refine the grains of magnesium alloys. However, these methods of adding alloy elements from outside have the following disadvantages: First, the way of adding elements Improper, prone to segregation or burning loss, lower yield, affecting the subsequent deformation of the alloy; second, the addition of precious elements increases the cost of the alloy
In addition, during the solidification process of the alloy, it is currently widely used to add an external field to achieve the purpose of refining the alloy structure, such as ultrasonic field, electromagnetic field, pulse field, etc., using the relevant principle of action to promote the breaking of large grains. However, these methods have the following disadvantages: first, the cost of equipment is relatively high, and the maturity of the process applied in magnesium alloy is not large; second, the range of action is very limited and it is easy to have the possibility of unevenness The range is limited by the power of the device

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Embodiment 1: 800Kg Mg-7Gd-5Y-1.0Ce-0.3Zr magnesium alloy homogenization and subsequent processing method.

[0035] The alloy obtained from the small sample has only one low-melting transformation point, which is 545°C. Heat the smelted ingot to 535°C±5°C with the furnace temperature rise, and keep it warm for 30 minutes; three-way forging on the forging press, the total deformation of forging is controlled within 30% by volume; the forged billet is put into homogenization heat treatment again In the furnace, keep warm for 16~20 hours; then out of the furnace, continue forging, the temperature after forging is not lower than 480°C, then extrude into bars, and finally water-cooled; artificially heat the bars at 220°C~250°C The aging time is 8~20h.

[0036] The method of the invention significantly improves the deformability of the alloy, and at the same time greatly shortens the homogenization time, improves the production efficiency, and reduces the preparation cost. ...

Embodiment 2

[0037] Example 2: Homogenization and subsequent processing of 800KgMg-8Gd-3Y-0.2Ca-0.6Zr magnesium alloy.

[0038]The alloy obtained from the small sample has only one low-melting transformation point, which is 540°C. After the alloy is smelted, it is cooled and solidified, and it is taken out when the surface temperature drops to 525°C; it is extruded on an extruder, and the total deformation is controlled within 30% by volume; the extruded alloy is placed in a homogenization heat treatment furnace for heat preservation , the temperature is set at 525°C±5°C, and the holding time is 16~24h; then the ingot is taken out and extruded directly without cooling, the extrusion is 20, and the extruded alloy is directly water-cooled; artificial aging is carried out, and the aging system The aging time is 8~20h at 220℃~250℃.

[0039] The method of the invention shortens the homogenization time of the alloy and improves the production efficiency at the same time, which is greatly improv...

Embodiment 3

[0040] Embodiment 3: 40KgAZ80 magnesium alloy homogenization and subsequent processing method.

[0041] The alloy obtained from the small sample has only one low-melting transformation point, which is 420°C. Use AZ80's own resistance for heating. After power on, AZ80 is equivalent to an electrical appliance. When the temperature control system shows that the temperature of the AZ80 billet is 415°C±5°C, keep it warm for 10~30min; roll the AZ80 alloy and control the deformation at 20% by volume About; put the billet back into the homogenization heat treatment furnace for homogenization heat treatment, the temperature is about 415°C±5°C, and the holding time is 16~24h; the material is taken out and three-way forging is carried out, and the forging temperature is controlled above 350°C. Then perform secondary extrusion, and the extruded material is directly water-cooled; artificial aging is performed, and the aging system is 8-20 hours at 140°C-200°C.

[0042] The method of the p...

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PUM

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Abstract

The invention discloses a homogenization treatment and subsequent processing method suitable for magnesium alloy ingots. The method comprises the following steps: (1) analyzing components of a magnesium alloy and number of low melting point phases; (2) performing the following steps according to the number of low melting point phases: preheating at a temperature which is 10-20 DEG C lower than an initial melting temperature of the low melting point phase change, performing deformation comprising one or a combination of optional two in forging, extruding and rolling on the alloy, and performing long-term homogenization on the deformed alloy; (3) performing subsequent alloy treatment, comprising the following sub-steps: performing direct ageing, continuously deforming and performing ageing, raising the temperature to 10-20 DEG C below the initial melting temperature of the next low melting point phase change, deforming, homogenizing, repeating until the low melting point phases are completely eliminated, and directly deforming and ageing without cooling after the homogenization is finished finally.

Description

technical field [0001] The invention relates to a method suitable for homogenization treatment and subsequent processing of magnesium alloys, which belongs to the category of industrial magnesium alloys. Background technique [0002] Due to its high specific strength, specific stiffness, and electromagnetic shielding properties, magnesium alloys are increasingly used in aerospace and other related fields. Aging strengthening, as one of the most important strengthening methods for magnesium alloys, is currently a research hotspot and difficulty both at home and abroad. As a common smelting and casting magnesium alloy, there are often a large number of undecomposed eutectic structures, which form relatively serious specific gravity segregation, especially For magnesium alloys with high alloy element content, this limits and reduces the subsequent aging strengthening effect of the alloy. Therefore, in order to improve the precipitation strengthening efficiency of the alloy, it ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22F1/06
Inventor 马鸣龙张奎李兴刚李永军石国梁袁家伟李婷廖洪彬
Owner GRIMAT ENG INST CO LTD
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