A glass substrate pretreatment method and a method for manufacturing solar cell encapsulation glass using it
A technology for solar cells and encapsulation glass, applied in the field of manufacturing solar cell encapsulation glass and glass substrate pretreatment, can solve the problem of poor hardness and friction resistance of anti-reflection coating, failure of anti-reflection function of anti-reflection coating, and adhesion of anti-reflection coating. Problems such as poor focus, to achieve the effect of good adhesion, good hardness and friction resistance of the anti-reflection coating, and low cost
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Embodiment 1
[0029] A kind of glass substrate pretreatment method, it comprises the following steps:
[0030] Step 1: Immerse the cleaned glass substrate in the mixed solution of concentrated sulfuric acid and hydrogen peroxide for 0.5h, take it out and then use deionized water for ultrasonic cleaning, and then put it in an oven to dry to obtain the surface hydroxylated glass substrate piece. In this embodiment, in the mixed solution of concentrated sulfuric acid and hydrogen peroxide, the volume ratio of concentrated sulfuric acid and hydrogen peroxide is 7:3. In the present invention, the concentrated sulfuric acid used is concentrated sulfuric acid with a mass fraction of 98%, and the hydrogen peroxide used is hydrogen peroxide with a mass fraction of 30%.
[0031] Step 2: Place the above-mentioned surface hydroxylated glass substrate in a mixed solution of 3-aminopropyltriethoxysilane and ethanol, let it stand for 5 hours, then take out the glass substrate and dry it with nitrogen, an...
Embodiment 2
[0033] A kind of glass substrate pretreatment method, it comprises the following steps:
[0034] Step 1: Immerse the cleaned glass substrate in the mixed solution of concentrated sulfuric acid and hydrogen peroxide for 1.5 hours, take it out and then use deionized water to perform ultrasonic cleaning, and then put it in an oven to dry to obtain the surface hydroxylated glass substrate. piece. In this embodiment, in the mixed solution of concentrated sulfuric acid and hydrogen peroxide, the volume ratio of concentrated sulfuric acid and hydrogen peroxide is 3:1.
[0035] Step 2: Place the above-mentioned surface hydroxylated glass substrate in a mixed solution of 3-aminopropyltriethoxysilane and ethanol, leave it to react for 7 hours, take out the glass substrate and dry it with nitrogen, and then put it in After drying in an oven at 100° C. for 40 minutes, cool to room temperature to obtain an aminated glass substrate, which is the pretreated glass substrate. In the present ...
Embodiment 3
[0037] A kind of glass substrate pretreatment method, it comprises the following steps:
[0038] Step 1: Immerse the cleaned glass substrate in the mixed solution of concentrated sulfuric acid and hydrogen peroxide for 1 hour, take it out and then perform ultrasonic cleaning with deionized water, and then put it in an oven to dry to obtain a glass substrate with hydroxylated surface . In this embodiment, in the mixed solution of concentrated sulfuric acid and hydrogen peroxide, the volume ratio of concentrated sulfuric acid and hydrogen peroxide is 3:2.
[0039]Step 2: Place the above-mentioned surface hydroxylated glass substrate in a mixed solution of 3-aminopropyltriethoxysilane and ethanol, let it stand for 6 hours, then take out the glass substrate and dry it with nitrogen, and then put it in After drying in an oven at 120° C. for 30 minutes, cool to room temperature to obtain an aminated glass substrate, which is the pretreated glass substrate. In the present embodimen...
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