Method for preparing nanometer copper through chemical reduction method
A technology of nano-copper powder and reducing agent, which is applied in the field of preparing nano-copper by chemical reduction method, which can solve the problems that the active metal powder reducing agent is not easy to clean and affects the purity of nano-copper powder.
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[0017] The preparation of nano copper powder is carried out according to the following steps:
[0018] (1) Dissolve 10g of copper sulfate in 300ml of deionized water, add 5g of polyacrylic acid, stir to dissolve it, and then add 150ml of ammonia water with a concentration of 25% to form a dark blue aqueous solution of tetraammonia copper complex ions
[0019] (2) Dissolve 5g of sodium hypophosphite in 20ml of water to obtain a homogeneous solution
[0020] (3) Pour solution (2) into (1). Stirring was continued, resulting in a precipitate, until the solution became colorless
[0021] (4), stop stirring and let it stand, remove the supernatant
[0022] (5) Wash twice with ethanol
[0023] (6) Treat the cleaned precipitate in (5) at 100°C for 10 hours under a nitrogen atmosphere to obtain nano-copper powder
[0024] The advantages of the present invention are:
[0025] (1) The present invention has high reduction efficiency and high recovery rate, and the nanometer particle ...
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