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Modified natural plant filter tip additive material capable of selectively reducing burst size of hydrogen cyanide in main stream smoke of cigarettes and preparation method of modified natural plant filter tip additive material

A technology of cigarette mainstream smoke and natural plants, applied in the field of modified natural plant filter additive materials and its preparation, can solve the problem of lack of selectivity in hydrogen cyanide removal, affecting the sensory quality of cigarettes, weak hydrogen cyanide adsorption capacity, etc. problems, to achieve the effects of reducing the hazards of cigarettes, low cost, and easy large-scale production

Active Publication Date: 2013-11-20
ZHENGZHOU TOBACCO RES INST OF CNTC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

CN101336752A directly adds or adsorbs alkaline substances in the fiber substrate, but lacks selectivity for the removal of hydrogen cyanide
To sum up, the current research has a certain effect on reducing the release of hydrogen cyanide in the mainstream smoke of cigarettes, but there are also problems such as weak selective adsorption of hydrogen cyanide, affecting the sensory quality of cigarettes, and the cost of harm reduction materials is expensive and difficulty in industrialization and many other problems, so it has not really been widely used

Method used

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  • Modified natural plant filter tip additive material capable of selectively reducing burst size of hydrogen cyanide in main stream smoke of cigarettes and preparation method of modified natural plant filter tip additive material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Example 1. Wash, degas, dry, pulverize and sieve Radix Radix to prepare (20 mesh-100 mesh) granules; add 10g of Radix Radix to 30g of anhydrous pyridine, then slowly add 10g of succinic anhydride, and after reflux for 5 hours, Cool to room temperature, filter with suction and wash with anhydrous pyridine, dry at 60°C for 12 hours, and sieve to select product particles of 20 mesh to 100 mesh. Take 5 g of the carboxylated product, add it to 100 mL of 0.2 mol / L ferric chloride aqueous solution, react at room temperature for 4 hours, dehydrate, wash with water, dry at 60°C for 12 hours, sieve, and select product particles of 20 mesh to 100 mesh to obtain materials needed.

Embodiment 2

[0019] Example 2. Wash the poria cocos, remove impurities, dry, pulverize and sieve to prepare (20 mesh-100 mesh) granules; add 10g of poria cocos granules to 40g of anhydrous pyridine, then slowly add 20g of maleic anhydride, and reflux reaction After 6 hours, cool to room temperature, filter with suction and wash with anhydrous pyridine, dry at 60°C for 12 hours, and sieve to select product particles of 20 mesh to 100 mesh. Take 5 g of the carboxylated product, add it to 200 mL of 0.1 mol / L ferric sulfate aqueous solution, react at room temperature for 5 hours, dehydrate, wash with water, dry at 60°C for 12 hours, sieve, and select 20 mesh-100 mesh product particles to obtain the obtained Need materials.

Embodiment 3

[0020] Example 3. Remove the sponge from the corn cob, wash, remove impurities, dry, crush and sieve to prepare (20 mesh-100 mesh) granules; add 10g corn cob granules to 50g anhydrous pyridine, and then slowly add 20g Phthalic anhydride, after reflux reaction for 5 hours, cooled to room temperature, suction filtered and washed with anhydrous pyridine, dried at 60°C for 12 hours, sieved, and selected 20 mesh-100 mesh product particles. Take 5 g of the carboxylated product, add it to 200 mL of 0.15 mol / L copper sulfate aqueous solution, react at room temperature for 4 hours, dehydrate, wash with water, dry at 60°C for 12 hours, sieve, and select 20-100 mesh product particles to obtain the obtained Need materials.

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Abstract

The invention discloses a modified natural plant filter tip additive material capable of selectively reducing burst size of hydrogen cyanide in main stream smoke of cigarettes and a preparation method of the modified natural plant filter tip additive material. The modified natural plant filter tip additive material takes the natural plant material as a carrier and is prepared through carboxylation and loading of transition metal ions sequentially. According to the invention, the filter tip additive material prepared by taking the natural plant material as the carrier has the porous adsorption property and is rich in transition metal ions; as CN- has strong complexation to the transition metal ions, the filter tip additive material can perform effective adsorption and complexation on hydrogen cyanide, and the purpose of selectively reducing burst size of hydrogen cyanide in main stream smoke of cigarettes is realized. According to the modified natural plant filter tip additive material and the preparation method, the source of the raw material is extensive, green and environmentally friendly; the prepared filter tip additive material is high in safety, simple in preparation technology, low in cost, and easy to produce on a large scale; when applied to cigarette filter tips, the modified natural plant filter tip additive material can selectively reduce burst size of hydrogen cyanide in main stream smoke of cigarettes by more than 35% with no negative effect on the sensory quality of cigarettes.

Description

[0001] technical field [0002] The invention belongs to the technical field of cigarettes, and relates to a modified natural plant filter additive material for selectively reducing the hydrogen cyanide release in mainstream smoke of cigarettes and a preparation method thereof. Applying the material to cigarette filter rods can effectively and selectively reduce the amount of hydrogen cyanide released in mainstream smoke of cigarettes without negatively affecting the sensory quality of cigarettes. Background technique [0003] Hydrogen cyanide is an important harmful component in cigarette smoke and one of the seven representative harmful components in mainstream cigarette smoke. All phases are distributed, and the gas / particle ratio is generally greater than 1:1. Hydrogen cyanide is the most toxic substance in cigarette smoke. Hydrogen cyanide in the smoke quickly enters the body after being absorbed by the respiratory tract, causing harm to human health. Therefore, it is...

Claims

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Application Information

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IPC IPC(8): A24D3/06
Inventor 王宜鹏聂聪赵乐孙培健孙学辉贾云祯杨松彭斌刘惠民
Owner ZHENGZHOU TOBACCO RES INST OF CNTC
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