Phosphorus removal adsorbent for loading composite metal via active carbon fiber and preparation method of phosphorus removal adsorbent
A technology of activated carbon fibers and composite metals, which is applied in the fields of alkali metal compounds, chemical instruments and methods, adsorption water/sewage treatment, etc., can solve the problems of low phosphorus affinity, rare earth materials are not easy to obtain in large quantities, and are expensive. The preparation method is novel and simple, the preparation process time is short, and the effect of excellent adsorption performance
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Embodiment 1
[0019] Embodiment one: the concrete steps of this embodiment are:
[0020] a. Prepare 10 mL of a mixed solution of ferric nitrate and lanthanum nitrate with a total molar concentration of 0.1 mol / L with the molar ratio of iron-lanthanum ions at 1:9.
[0021] b. Cut the activated carbon fibers into 0.4-0.6cm cubes, wash with water for several times, soak in deionized water, filter and dry;
[0022] c. Weigh 0.2 g of the activated carbon fiber obtained in step b, add it to the suspension obtained in step a, soak for 10 min, and filter;
[0023] d. After drying the solid obtained in step c at 105°C, activate it with a muffle furnace at 650°C for 120 minutes; wait until it cools down to room temperature to obtain the adsorbent, and keep it sealed.
[0024] The adsorption capacity data of the composite phosphorus removal adsorbent in this example are shown in Table 1.
Embodiment 2
[0025] Embodiment 2: The technical solution of this embodiment is basically the same as that of Embodiment 1, the difference lies in:
[0026] In step a, 10 mL of a mixed solution of ferric nitrate and lanthanum nitrate with a total molar concentration of 0.1 mol / L was prepared with an iron-lanthanum ion molar ratio of 3:7. The adsorption capacity data of the composite phosphorus removal adsorbent in this example are shown in Table 1.
Embodiment 3
[0027] Embodiment 3: The technical solution of this embodiment is basically the same as that of Embodiment 1, the difference lies in:
[0028] In step a, 10 mL of a mixed solution of ferric nitrate and lanthanum nitrate with a total molar concentration of 0.1 mol / L was prepared with an iron-lanthanum ion molar ratio of 1:1. The adsorption capacity data of the composite phosphorus removal adsorbent in this example are shown in Table 1.
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