Preparation method of high-resistance polymer coating liquid
A technology of high molecular polymer and coating liquid, applied in the directions of starch derivative coatings, cellulose derivative coatings, coatings, etc., can solve the problems of difficult recycling and difficult processing of polymer materials, so as to reduce processing costs and prepare Simple method and simple equipment requirements
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Embodiment 1
[0048] High barrier polymer coating solution includes the following components:
[0049] Polyvinyl alcohol PVOH 18wt%, its molecular weight is 13200, alcoholysis degree is 88wt%;
[0050] Nano silica 1wt%, specific surface area is 200m 2 / g;
[0051] Silane coupling agent KH-570 0.1%wt;
[0052] Acetic acid 0.32wt%;
[0053] Polyacrylic acid 0.32wt%, its molecular weight 5000;
[0054]Cross-linking agent 1.2wt%, described cross-linking agent is the mixture of boric acid and sodium borate, and its weight ratio is 1: 1;
[0055] Ethanol 5wt%;
[0056] Water 74.06wt%.
[0057] The preparation method of the above-mentioned high barrier polymer coating liquid is:
[0058] (1) Add 25 parts of PVOH with a molecular weight of 13200 and an alcoholysis degree of 88%wt to 75 parts of water at 92°C, stir at 500 rpm for 40 minutes to obtain a solution, cool to 30°C for use.
[0059] (2) The specific surface area of 25 parts is 200m 2 / g silicon dioxide, 2.5 parts of KH-570, 3.5 ...
Embodiment 2
[0063] High barrier polymer coating solution includes the following components:
[0064] Polyvinyl alcohol PVOH 10.5wt%, its molecular weight 75000, alcoholysis degree 99%wt;
[0065] Nano silicon dioxide 3.6wt%, specific surface area is 200m2 / g;
[0066] Silane coupling agent KH-570 0.05%wt;
[0067] Acetic acid 1.325wt%;
[0068] Polymethacrylic acid 1.2wt%, its molecular weight 5000;
[0069] Cross-linking agent 0.45wt%, described cross-linking agent is the mixture of boric acid and sodium borate, and its weight ratio is 1: 1;
[0070] Isopropanol 8wt%;
[0071] Water 74.875wt%.
[0072] The preparation method of the above-mentioned high barrier polymer coating liquid is:
[0073] (1) Add 20 parts of PVOH with a molecular weight of 75,000 and an alcoholysis degree of 99% wt to 80 parts of water at 92°C, stir at 800 rpm for 40 minutes to obtain a solution, cool to 30°C for later use;
[0074] (2) The specific surface area of 24 parts is 200m 2 / g silicon dioxide, 0...
Embodiment 3
[0078] High barrier polymer coating solution includes the following components:
[0079] Polyvinyl alcohol PVOH 10wt%, its molecular weight 75000, alcoholysis degree 99%wt;
[0080] Nano-alumina 7wt%, specific surface area is 200m 2 / g;
[0081] Acetic acid 1.18wt%;
[0082] Polymethacrylic acid 0.168wt%, its molecular weight 5000;
[0083] Cross-linking agent 0.5wt%, described cross-linking agent is the mixture of boric acid and sodium borate, and its weight ratio is 1: 3;
[0084] Isopropanol 11.72wt%;
[0085] Water 69.432wt%.
[0086] The preparation method of the above-mentioned high barrier polymer coating liquid is:
[0087] (1) Add 20 parts of PVOH with a molecular weight of 75000 and an alcoholysis degree of 99%wt to 80 parts of water at 95°C, stir at 800rpm for 40 minutes to obtain a solution, cool to 30°C for later use;
[0088] (2) The specific surface area of 25 parts is 200m 2 / g alumina, 3.5 parts of acetic acid, 0.6 part of 10000 molecular weight poly...
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