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Preparation method of efficient dephosphorizing porous particle adsorbent

A particulate adsorbent and porous technology, which is applied in the field of preparation of high-efficiency phosphorus removal porous particulate adsorbent, can solve the problems of difficult recovery, equipment blockage and high production cost, and achieves high adsorption efficiency, wide applicability and simple production process. Effect

Active Publication Date: 2014-03-26
北京涞澈科技发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] However, the adsorbent prepared by the above-mentioned patents has the problems of easily causing equipment blockage, not being easy to recover phosphorus resources, and high production costs.
To a certain extent, the application of phosphorus removal by adsorption is limited.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Dolomite clay and montmorillonite clay were purchased from Zhenyongwei Technology Co., Ltd., the raw materials were crushed to 200 mesh, and 3g of dolomite powder, 3g of montmorillonite powder, 2g of soluble starch, 2g of Al 2 (SO4) 3 Put the powder into the blender, slowly add an appropriate amount of water, and stir evenly; knead the evenly stirred material into uniform spherical particles with a diameter of 3~5mm; place the shaped particles in an oven at 105°C for 24 hours and then place them in a muffle furnace Roasting at 600°C for 1 hour, and then cooling down to room temperature naturally, a porous particle adsorbent with high efficiency for phosphorus removal was prepared.

[0024] Weigh 0.5g of the high-efficiency phosphorus removal porous particle adsorbent prepared above, put it into a 250mL Erlenmeyer flask, add 100mL of simulated wastewater solution containing 10mg / L phosphorus, without stirring, and let it stand at a constant temperature of 20°C±1°C for 12...

Embodiment 2

[0027] Dolomite clay and montmorillonite clay were purchased from Zhenyongwei Technology Development Co., Ltd., and the raw materials were crushed to 160 mesh, and 1 g of dolomite powder, 1 g of montmorillonite powder, 2 g of soluble starch, and 2 g of Al 2 (SO4) 3 Put the powder into a mixer, slowly add an appropriate amount of water, and stir evenly; knead the evenly stirred material into uniform spherical particles with a diameter of 3 mm; place the shaped particles in an oven for 20 hours at 100 °C and then place them in a muffle furnace Calcined at 650°C for 0.8 h, then cooled down to room temperature naturally, and a porous granular adsorbent with high efficiency for phosphorus removal was prepared.

[0028] Weigh 0.5 g of the high-efficiency phosphorus removal porous particle adsorbent prepared above and place it in a 250 mL Erlenmeyer flask, add 100 mL of simulated wastewater solution containing 20 mg / L phosphorus, without stirring, and let it stand at a constant tempe...

Embodiment 3

[0031] Dolomite clay and montmorillonite clay were purchased from Zhenyongwei Technology Development Co., Ltd., and the raw materials were crushed to 180 mesh, and 2 g of dolomite powder, 2 g of montmorillonite powder, 2 g of soluble starch, and 2 g of Al 2 (SO4) 3 Put the powder into the blender, slowly add an appropriate amount of water, and stir evenly; knead the evenly stirred material into uniform spherical particles with a diameter of 5 mm; place the shaped particles in an oven for 18 hours at 120°C and then place them in a muffle furnace Calcined at 550°C for 1.2 h, and then cooled down to room temperature naturally, the highly efficient phosphorus removal porous particle adsorbent was prepared.

[0032] Weigh 0.5 g of the high-efficiency phosphorus-removing porous particle adsorbent prepared above and place it in a 250 mL conical flask, add 100 mL of simulated wastewater solution containing 50 mg / L phosphorus, without stirring, and place it under constant temperature c...

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Abstract

The invention discloses a preparation method of an efficient dephosphorizing porous particle adsorbent. The method comprises the following steps of: (1) preparing raw materials: preparing dolomite clay and montmorillonite clay serving as raw materials; (2) granulating and casting: adding water, soluble starch and Al2(SO4)3 into the dolomite clay and montmorillonite clay serving as raw materials, fully and uniformly stirring, granulating, casting and drying; and (3) sintering. In the method, a production process is simple, production cost is low, and harm gases and sewage are not produced in a production process. The prepared adsorbent has high affinity to water body phosphorus, has high adsorption efficient, does not poison water bodies or aquatic organisms, and can be removed from water bodies conveniently after use. The prepared adsorbent has high adaptability on the aspect of phosphorus removal from phosphorus-containing water bodies, and can be applied to removal of phosphorus from industrial waste water, domestic sewage, agricultural runoff and other natural water bodies.

Description

technical field [0001] The invention relates to a preparation method of an adsorbent for sewage treatment, in particular to a preparation method of a highly efficient phosphorus removal porous particle adsorbent. Background technique [0002] The per capita possession of water resources in my country is small, and the spatial distribution is unbalanced. With the acceleration of urbanization and industrialization in my country, the demand gap for water resources is also increasing. At the same time, with the increase of urban population and the development of industrial and agricultural production, the amount of sewage discharge is also increasing, and the water pollution is quite serious, almost all over the country. In this context, the sewage treatment industry has become a new industry. [0003] Due to the high construction costs and operating costs of sewage treatment, many areas do not have a complete industrial wastewater and municipal domestic sewage treatment system...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J20/283B01J20/30C02F1/28
Inventor 陈男冯传平高雅
Owner 北京涞澈科技发展有限公司
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