Preparation method of efficient dephosphorizing porous particle adsorbent
A particulate adsorbent and porous technology, which is applied in the field of preparation of high-efficiency phosphorus removal porous particulate adsorbent, can solve the problems of difficult recovery, equipment blockage and high production cost, and achieves high adsorption efficiency, wide applicability and simple production process. Effect
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Embodiment 1
[0023] Dolomite clay and montmorillonite clay were purchased from Zhenyongwei Technology Co., Ltd., the raw materials were crushed to 200 mesh, and 3g of dolomite powder, 3g of montmorillonite powder, 2g of soluble starch, 2g of Al 2 (SO4) 3 Put the powder into the blender, slowly add an appropriate amount of water, and stir evenly; knead the evenly stirred material into uniform spherical particles with a diameter of 3~5mm; place the shaped particles in an oven at 105°C for 24 hours and then place them in a muffle furnace Roasting at 600°C for 1 hour, and then cooling down to room temperature naturally, a porous particle adsorbent with high efficiency for phosphorus removal was prepared.
[0024] Weigh 0.5g of the high-efficiency phosphorus removal porous particle adsorbent prepared above, put it into a 250mL Erlenmeyer flask, add 100mL of simulated wastewater solution containing 10mg / L phosphorus, without stirring, and let it stand at a constant temperature of 20°C±1°C for 12...
Embodiment 2
[0027] Dolomite clay and montmorillonite clay were purchased from Zhenyongwei Technology Development Co., Ltd., and the raw materials were crushed to 160 mesh, and 1 g of dolomite powder, 1 g of montmorillonite powder, 2 g of soluble starch, and 2 g of Al 2 (SO4) 3 Put the powder into a mixer, slowly add an appropriate amount of water, and stir evenly; knead the evenly stirred material into uniform spherical particles with a diameter of 3 mm; place the shaped particles in an oven for 20 hours at 100 °C and then place them in a muffle furnace Calcined at 650°C for 0.8 h, then cooled down to room temperature naturally, and a porous granular adsorbent with high efficiency for phosphorus removal was prepared.
[0028] Weigh 0.5 g of the high-efficiency phosphorus removal porous particle adsorbent prepared above and place it in a 250 mL Erlenmeyer flask, add 100 mL of simulated wastewater solution containing 20 mg / L phosphorus, without stirring, and let it stand at a constant tempe...
Embodiment 3
[0031] Dolomite clay and montmorillonite clay were purchased from Zhenyongwei Technology Development Co., Ltd., and the raw materials were crushed to 180 mesh, and 2 g of dolomite powder, 2 g of montmorillonite powder, 2 g of soluble starch, and 2 g of Al 2 (SO4) 3 Put the powder into the blender, slowly add an appropriate amount of water, and stir evenly; knead the evenly stirred material into uniform spherical particles with a diameter of 5 mm; place the shaped particles in an oven for 18 hours at 120°C and then place them in a muffle furnace Calcined at 550°C for 1.2 h, and then cooled down to room temperature naturally, the highly efficient phosphorus removal porous particle adsorbent was prepared.
[0032] Weigh 0.5 g of the high-efficiency phosphorus-removing porous particle adsorbent prepared above and place it in a 250 mL conical flask, add 100 mL of simulated wastewater solution containing 50 mg / L phosphorus, without stirring, and place it under constant temperature c...
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