Air filter material based on carbon nano tube and preparation method thereof
An air filter material and carbon nanotube technology, which is applied in the fields of filtration and separation, separation methods, chemical instruments and methods, etc., can solve the damage of the intrinsic properties of carbon nanotubes, affect the quality of carbon nanotube membranes, and increase the resistance of carbon nanotube membranes. Advanced problems, achieve good industrial application prospects, good strength, and avoid the effect of material size and shape limitations
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Embodiment 1
[0032] Example 1. Preparation of carbon nanotube air filter material based on quartz fiber filter medium
[0033] Quartz fiber filter media (such as figure 2 As shown in (a), the average diameter of the quartz fiber is 3 μm), which is placed in the heating section of the quartz sleeve (such as figure 1 The position shown in 6); take ferrocene as the catalyst, and place it at the mouth of the quartz tube (such as figure 1 The position shown in 3 in the middle), the temperature at the position of the catalyst in the reaction process is 120 ° C; with argon and hydrogen as protective atmosphere, ethylene as carbon source, the ratio is argon: hydrogen: ethylene=7: 1: 2, gas flow rate is 3 mm / s, the temperature is raised to 760 ° C, and the reaction is performed for 1 hour to obtain an air filter material based on carbon nanotubes, such as figure 2 As shown in (b), the average diameter of the carbon nanotubes is 25 nm.
[0034] The scanning electron microscope photo of the carb...
Embodiment 2
[0037] Example 2. Preparation of carbon nanotube air filter material based on carbon fiber filter medium
[0038] The carbon fiber filter medium (the average diameter of the carbon fiber is 5μm, in the form of a folded cloth) is placed in the heating section of the quartz sleeve (such as figure 1 The position shown in 6); take ferrocene as the catalyst, and place it at the mouth of the quartz tube (such as figure 1 The position shown in 3 in the middle), the temperature at the position of the catalyst in the reaction process is 120 ° C; with argon and hydrogen as protective atmosphere, ethylene as carbon source, the ratio is argon: hydrogen: ethylene=7: 1: 2, gas flow rate is 3 mm / s, the temperature is raised to 850° C., and the reaction is performed for 15 minutes to obtain an air filter material based on carbon nanotubes, and the average diameter of the carbon nanotubes is 25 nm.
Embodiment 3
[0039] Example 3. Preparation of carbon nanotube air filter material based on the folded quartz fiber filter medium
[0040] Place the folded quartz fiber filter medium (the average diameter of the quartz fiber is 3 μm) in the heating section of the quartz sleeve (such as figure 1 The position shown in 6); take ferrocene as the catalyst, and place it at the mouth of the quartz tube (such as figure 1 The position shown in 3 in the middle), the temperature at the position of the catalyst in the reaction process is 120 ° C; with argon and hydrogen as protective atmosphere, ethylene as carbon source, the ratio is argon: hydrogen: ethylene=7: 1: 2, gas flow rate is 3 mm / s, the temperature is raised to 760° C., and the reaction is performed for 1 hour to obtain an air filter material based on carbon nanotubes, and the average diameter of the carbon nanotubes is 25 nm.
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