Application of high dielectric constant materials in preparation of dielectric magnetic multiple device
A high dielectric constant and versatile technology, applied in the field of high dielectric constant materials in the preparation of dielectric magnetic composite devices, can solve the problem of low dielectric constant, heterogeneous co-firing of ferrite materials, and low cut-off frequency EMI filter and other issues, to achieve good dielectric temperature properties, good insulation properties, low dielectric loss effect
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Embodiment 1
[0045] Weigh each powder according to the weight ratio given by the formula number A1 in Table 1: BaTiO 3 : 100.0 g, Bi 2 o 3 : 6.0 g, CuO: 2.0 g, low-melting glass: 2.0 g.
[0046] where BaTiO 3 It is an electronic grade raw material with a purity of at least 99.0% and a particle size D50≤1.0μm.
[0047] Among them Bi 2 o 3 It is an electronic grade raw material with a purity of at least 99.5% and a particle size D50≤5.0μm.
[0048] Among them, CuO is an analytically pure raw material with a purity of at least 99.0% and a particle size D50≤3.0μm.
[0049] Among them, the melting point of the low-melting point glass is lower than 800°C, and the particle size D50≤2.5μm.
[0050] The preparation method of the high dielectric constant low temperature co-fired ceramic material in this embodiment is as follows:
[0051] 1) Ball milling and mixing
[0052] BaTiO 3 、 Bi 2 o 3 , CuO and low-melting glass are mixed according to the above weight, and add 120 grams of deioniz...
Embodiment 2
[0059] Take each powder according to the weight ratio given by the formula number A2 in Table 1: BaTiO 3 : 100.0 g, Bi 2o 3 : 6.0g, CuO: 2.0g, low melting point glass: 2.5g, MnCO 3 : 0.2 g.
[0060] where BaTiO 3 、 Bi 2 o 3 , CuO and low-melting glass raw material requirements are the same as in Example 1, and the MnCO 3 It is a chemically pure raw material, and its content (calculated as Mn) is not less than 44.0%.
[0061] The preparation method of the high dielectric constant low temperature co-fired ceramic material in this embodiment is as follows:
[0062] 1) Ball milling and mixing
[0063] BaTiO 3 、 Bi 2 o 3 , CuO, low melting glass and MnCO 3 Mix according to the above weight, and add 120 grams of deionized water ball mill to obtain the ceramic material mixture;
[0064] 2) Dry the ball-milled ceramic material mixture
[0065] Dry the ceramic material mixture at a temperature of 150°C for 24 hours;
[0066] 3) Screening
[0067] The dried ceramic mater...
Embodiment 3
[0070] Take each powder according to the weight ratio given by the formula number A3 in Table 1: BaTiO 3 : 100.0 g, Bi 2 o 3 : 6.0g, CuO: 2.0g, low melting point glass: 3.0g, MnCO 3 : 0.2 g.
[0071] where BaTiO 3 、 Bi 2 o 3 , CuO, low melting glass and MnCO 3 Raw material requirement is identical with embodiment 2.
[0072] The preparation method of the high dielectric constant low temperature co-fired ceramic material in this embodiment is as follows:
[0073] 1) Ball milling and mixing
[0074] BaTiO 3 、 Bi 2 o 3 , CuO, low melting glass and MnCO 3 Mix according to the above weight, and add 120 grams of deionized water ball mill to obtain the ceramic material mixture;
[0075] 2) Dry the ball-milled ceramic material mixture
[0076] Dry the ceramic material mixture at a temperature of 150°C for 24 hours;
[0077] 3) Screening
[0078] The dried ceramic material mixture is separated by a 100-mesh screen to obtain a finished powder body of high dielectric cons...
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