System and method for measuring nitric oxide in a small amount of gas

A nitric oxide, a small amount of technology, used in measuring devices, instruments, scientific instruments and other directions, can solve problems such as insufficiency and large sample volume, and achieve the effect of small sample volume and high measurement accuracy

Inactive Publication Date: 2014-04-30
中科信蓝环保有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The currently widely used chemiluminescence method for measuring nitric oxide is an online detection device. The sample gas flow rate must be maintained at 800-1000 ml per minute or even higher, and continuous sample input is required. It takes at least 5-10 minutes to obtain a stable test data. liter sample volume, which is not possible for samples from ecosystem emissions
In particular, the culture experiments in some laboratories cannot meet such a large sample volume

Method used

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  • System and method for measuring nitric oxide in a small amount of gas
  • System and method for measuring nitric oxide in a small amount of gas
  • System and method for measuring nitric oxide in a small amount of gas

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Embodiment 1

[0034] Embodiment 1: as figure 1 The system for measuring nitric oxide in a small amount of gas samples of the present invention is shown, the system includes a first-stage sampling unit, a second-stage sampling unit, a reaction unit and a detection unit, wherein:

[0035] The first-stage sampling unit introduces a quantitative gas sample; the reaction unit is connected to the first-stage sampling unit, and the reaction unit receives the gas sample, and the gas sample reacts photochemically with the reaction gas provided by the reaction unit in the reaction unit under ultraviolet light irradiation , the reactant is generated after the reaction is sufficient, and the reactant generated by the reaction is pushed out by the piston of the reaction unit; the second-stage sampling unit is connected to the reaction unit, and the second-stage sampling unit receives the reactant generated by the reaction and enters the second quantitative tube. Carry out re-quantification, and then out...

Embodiment 2

[0067] Embodiment 2: as image 3 Shown is an embodiment of a measurement system for simultaneously measuring nitric oxide in a small amount of gas samples, including an analysis unit and a drive unit, and adopts the following technical solutions.

[0068] Analysis Department: It is composed of the first-stage sampling unit, the reaction unit, the second-stage sampling unit, and the detection unit. The gas sample enters the sampling unit through a syringe; the sampling unit is connected to the reaction unit through a stainless steel pipeline, and through the change of the state of the pneumatic valve of the sampling unit, the gas sample enters the reaction unit under the drive of high-purity nitrogen for photochemical reaction; the reaction unit and the second The secondary sampling unit is connected by a stainless steel pipeline, and the reactants generated by the reaction enter the second-level sampling unit for quantitative loading; the second-level sampling unit is connecte...

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Abstract

The invention discloses a system and method for measuring nitric oxide in a small amount of gas. The system and the method are used for measuring a trace of nitric oxide in the gas sample. The ppbv (parts per billion by volume)-level concentration can be detected by the system by using only milliliters of gas sample. The system comprises sample instruction units, a reaction unit and a detection unit. The analysis procedures are as follows: the quantitative gas sample introduced by the sample instruction units is delivered into the reaction unit and mixed the reaction gas provided by the system; at the same time, the ultraviolet light source in the system emits ultraviolet light, and the gas sample is subjected to chemical reaction to produce another reaction product which can be very easily detected by the detection unit; and after the reaction finishes, a piston of the reaction unit pushes the reaction product into the detection unit. Due to the high efficiency of reaction, the detected concentration of the reaction product and the concentration of the nitric oxide have linear corresponding relationship, thus after the concentration of the reaction product is calculated through the generation of signals of the reaction product in the detection unit, and the concentration of the nitric oxide in the gas sample can be calculated.

Description

technical field [0001] The invention relates to a system and method for measuring the concentration of nitric oxide in a small amount of gas, which is suitable for meteorological and environmental departments to monitor the concentration of nitric oxide in ecological system emission sources or for scientific research units to use for nitric oxide concentration in other emission sources Emission measurement. Background technique [0002] Nitric oxide is not only an indirect greenhouse gas, but also an important air pollutant component; it and volatile ammonia (NH3) in the ecosystem indirectly have an important impact on climate and ecological environment by promoting the formation of aerosol particles and other processes. Nitric oxide emitted by terrestrial ecosystems is transported and deposited through the atmosphere, which can not only affect nearby ecosystems, but also affect the carbon and nitrogen cycle and gas emission process of marine ecosystems. Since nitrogen-cont...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/02G01N30/20
Inventor 孙扬吉东升王跃思
Owner 中科信蓝环保有限公司
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