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Testing device for simulating equipment corrosion of continuous distillation industrial device

A test device and equipment corrosion technology, which is applied in the direction of measuring devices, weather resistance/light resistance/corrosion resistance, instruments, etc., can solve the problems of insufficient understanding of the characteristics of the vacuum distillation process, high content of colloidal asphaltenes, and few light components

Active Publication Date: 2013-04-10
CHINA PETROLEUM & CHEM CORP +1
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  • Abstract
  • Description
  • Claims
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Problems solved by technology

Heavy crude oil has high acid value, less light components, high density and viscosity, high colloidal asphaltene content, high salt content and heavy metal content, which seriously corrodes oil refining equipment, especially crude oil primary processing equipment, such as atmospheric and vacuum distillation units Directly subject to severe corrosion impact, but the industry has few ways to deal with it. The most important reason is the lack of understanding of the characteristics of the vacuum distillation process

Method used

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  • Testing device for simulating equipment corrosion of continuous distillation industrial device

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Embodiment Construction

[0023] See figure 1 , This test device mainly includes continuous distillation system, pressure control system, and corrosion sample system. The continuous distillation system includes a multi-necked flask 1, a main reactor 3, and a main condenser 7, the pressure control system includes a non-condensable gas receiving tank 10, a cold trap 11, a vacuum pump 19, and the corrosion sample system includes a vapor Sample coupon device for placing samples in phase and liquid phase. The multi-neck flask 1 is used to contain experimental media, such as crude oil after electro-desalination or atmospheric distillation column bottom oil. An electric heater (not shown) conforming to the shape of the multi-necked flask 1 is provided on the outside of the multi-necked flask 1 to heat the test medium in the flask. The main interface of the upper part of the multi-necked flask is connected with a glass cylindrical main reactor 3. The upper opening of the main reactor 3 is connected to a doub...

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Abstract

The invention relates to a testing device for simulating the equipment corrosion of a continuous distillation industrial device. The testing device comprises a continuous distillation system, a pressure control system and a corrosion sample system, wherein the top interface of a multi-mouth flask is connected with the bottom of a main reactor; the top interface of the main reactor is connected with the bottom of a main condenser; the top of the main condenser is connected with a non-condensable gas receiving tank, a cold trap, a gas buffering tank and an exhaust system through connecting pipes respectively, and is connected to a vacuum pump through the cold trap; and the corrosion sample system comprises a sample hanging device for placing samples into a steam phase and a liquid phase. A skillful reflow design is adopted in the invention, so that a condensed low-boiling-point liquid does not flow through the high-temperature main reactor, so that re-vaporization before reflowing to the bottom of the multi-mouth flask is avoided. Under the action of a reflow bypass, condensed low-boiling-point components and high-boiling-point components left at the bottom of the multi-mouth flask are fully mixed forcedly, and the distillation process is started once again, so that accurate simulation of continuous distillation is realized.

Description

Technical field [0001] The invention relates to an equipment corrosion test device that simulates a continuous distillation industrial device in a petroleum refining process. Background technique [0002] Atmospheric and vacuum distillation is the most important chemical separation process in the primary processing of petroleum refining. With the deterioration of crude oil worldwide, the main manifestation is the increase in acid content and the increase in the proportion of heavy crude oil. Heavy crude oil has high acid value, few light components, high density and viscosity, high colloidal asphaltene content, high salt content and heavy metal content, which is severely corroded to refinery equipment, especially primary crude oil processing equipment, such as atmospheric and vacuum distillation equipment It is directly affected by severe corrosion, and the industry does not have many methods for this. The most important reason is the lack of understanding of the characteristics...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N17/00
Inventor 屈定荣刘小辉蒋秀
Owner CHINA PETROLEUM & CHEM CORP
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