A surface-active amine preservative for thermal power plant boiler shutdown protection
A technology of active amines and preservatives, applied in the field of surfactants, can solve the problems of being easily broken, difficult to recover and analyze, affecting the stable operation of polishing treatment, etc., and achieve the effect of effective protection.
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Embodiment 1
[0008] Embodiment 1: every liter of surfactant amine preservative contains 1 mg of hydrazine, 200 μg of ethanolamine, 30 μg of hexamethylenetetramine, 3 mg of N-(2-aminoethyl) morpholine, 50 μg of pyrazine and 60 μg piperazine, ammonia water to adjust the pH value to 9.3, and the solvent of the surface active amine preservative is desalted water or deionized water. Low temperature test at 50°C. Put the test piece processed by the boiler water wall tube into the liquid phase and vapor phase of the deionized water containing the protective agent under the condition of 50°C for 2 hours to form a film at the same time. Take out the test piece and place it in a humid heat box together with the untreated test piece for 60 days. The corrosion rates of the test pieces are: 0.0023g / (m 2 h); Vapor-phase film-forming test piece 0.0031g / (m 2 h); untreated test piece 0.3608g / (m 2 h).
Embodiment 2
[0009] Embodiment 2: every liter of surface-active amine preservatives contains 4 mg of hydrazine, 380 μg of ethanolamine, 80 μg of hexamethylenetetramine, 9 mg of N-(2-aminoethyl) morpholine, 30 μg of pyrazine and 50 μg piperazine, ammonia water to adjust the pH value to 9.6, and the solvent of the surface active amine preservative is desalted water or deionized water. Medium temperature test at 150°C. Put the test piece processed by the boiler water wall tube into the autoclave, and under the condition of 150°C, film is formed simultaneously in the liquid phase and vapor phase of the deionized water containing the protective agent for 2 hours. Take out the test piece and place it in a humid heat box together with the untreated test piece for 60 days. The corrosion rates of the test pieces are: 0.0016g / (m 2 h); Vapor-phase film-forming test piece 0.0026g / (m 2 h); untreated test piece 0.3251g / (m 2 h).
Embodiment 3
[0010] Embodiment 3: every liter of surfactant amine preservative contains 2 mg of hydrazine, 260 μg of ethanolamine, 20 μg of hexamethylenetetramine, 7 mg of N-(2-aminoethyl) morpholine, 160 μg of pyrazine and 100 μg piperazine, ammonia water to adjust the pH value to 9.4, and the solvent of the surface active amine preservative is desalted water or deionized water. Medium temperature test at 250°C. The test piece processed by the boiler water wall tube is placed in an autoclave, and at 250°C, the film is formed simultaneously in the liquid phase and vapor phase of deionized water containing the protective agent for 2 hours. Take out the test piece and place it in a humid heat box together with the untreated test piece for 60 days. The corrosion rates of the test pieces are: 0.0011g / (m 2 h); Vapor-phase film-forming test piece 0.0015g / (m 2 h); untreated test piece 0.3417g / (m 2 h).
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