Alkaloid composite filter tip addition material capable of reducing hydrocyanic acid in cigarette mainstream smoke
A technology of cigarette mainstream smoke and additive materials, applied in e-liquid filter elements, tobacco, food science, etc., can solve the problems of reducing the release of hydrocyanic acid, which has not been reported, and achieve the effect of rapid and stable adsorption capacity
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[0016] General preparation method of the present invention is as follows:
[0017] 1. Combining one or more Chinese herbal medicines in the above-mentioned Coptis chinensis, Phellodendron phellodendri, three needles, and Huangtian bamboo in any proportion as the extraction raw material of plant alkaloids, extracting the alkaloids by acid water extraction, and drying them by crystallization Made into powder.
[0018] 2. Heat the alkaloid additive to 0.01% to 0.1% (mass percentage) sodium hydroxide solution to dissolve at 40°C. The amount of alkaloid dissolved is 0.1% to 15% of the weight of the activated carbon fiber carrier in advance.
[0019] 3. Put the activated carbon fiber in the 40°C solution prepared in Embodiment 3, soak it at a constant temperature and stir it for 1-2 hours, filter and wash it, and dry it in an oven at 60-100°C for 1-2 hours to obtain the activated carbon fiber loaded with alkaloids Material.
[0020] 4. Add the prepared filter tip additive material...
Embodiment 1
[0023] The specification 1 (specific surface area 1250m 2 / g,) of viscose-based activated carbon fiber is used as a composite filter additive material, loaded with 10% of the selected activated carbon fiber weight Phellodendron alkaloid, and then heated to 40 Dissolve at ℃, use activated carbon fiber of specification 1 to absorb alkaloids in the solution, filter, and dry. The amount of activated carbon fiber material added is 20 mg / cig. Cigarettes without any filter modification materials are used as reference products, and smoked according to the standard Conditions The cigarette smoking test was carried out on a smoking machine, and the amount of hydrocyanic acid released was tested according to the standard YC / T 253-2008, and the amount of tar was tested according to the standard GB / T 19609-2004. Two parallel samples were taken for each sample, and the results are shown in Table 1.
[0024] Table 1 The results of material 1 reducing the amount of hydrocyanic acid released ...
Embodiment 2
[0028] The specification 2 (specific surface area 1500m 2 / g) of viscose-based activated carbon fiber is used as a composite filter additive material, and the load is selected from alkaloids with 12% weight of activated carbon fibers. After mixing in proportion, extract plant alkaloids, heat the extracted alkaloids with 0.01% to 0.1% (mass percentage) sodium hydroxide solution to 40°C to dissolve, use specification 2 activated carbon fibers to absorb the alkaloids in the solution, filter ,dry. The dosage of the activated carbon fiber material is 18 mg / cig, and the cigarette without any filter modified material is used as the reference substance, and the cigarette smoking test is carried out on the smoking machine according to the standard smoking conditions, and according to the standard YC / T 253- In 2008, the release of hydrocyanic acid was tested, and the amount of tar was tested according to the standard GB / T 19609-2004. There were two parallel samples for each samp...
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