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Solvent-based fluorocarbon resin

A fluorocarbon resin, solvent-based technology, applied in the field of fluorocarbon resin synthesis technology, can solve the problems of high production cost, low product yield, long production cycle, etc., and achieve short production cycle, high transparency and low surface tension. Effect

Inactive Publication Date: 2010-09-22
徐州中研科技工业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, people still produce fluorocarbon resin through traditional synthesis process polymerization, the traditional synthesis process has a long production cycle, generally takes 72 hours to complete; after the polymerization reaction, the product yield is low, only reaching 85%, and the production cost is high; chemical substances, causing a lot of pollution to the environment and wasting a lot of resources

Method used

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  • Solvent-based fluorocarbon resin
  • Solvent-based fluorocarbon resin

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Embodiment 1

[0027] Embodiment 1: According to chlorotrifluoroethylene monomer 38.56%, methyl isobutyl (methyl) ketone 10.44%, xylene 24.38%, azobisisobutyronitrile 0.832%, undecylenic acid 1.024%, allyl alcohol The ratio of 2.894%, vinyl acetate 21.87% by mass percentage; the English abbreviation of chlorotrifluoroethylene monomer is CTFE, and the English abbreviation of methyl isobutyl (methyl) ketone is MIBK;

[0028] The synthesis process of solvent-based fluorocarbon resin: preparation---add raw materials to the polymerization kettle---vacuumize the polymerization kettle---add monomer chlorotrifluoroethylene raw materials to the polymerization kettle---stir, heat--- -Discharge;

[0029] 1. Preparation:

[0030] (1) Carry out pressure experiment to polymerization kettle, pressure 1Mpa, after holding pressure for 6 hours, release pressure for standby;

[0031] (2) Check the oil level of the reducer oil window of the stirring motor, the oil level of the vacuum pump oil level window and...

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Abstract

The invention provides a solvent-based fluorocarbon resin, belonging to the synthesis process of the fluorocarbon resin. The fluorocarbon resin comprises the following components by mass percent: 38.56% of a chlorotrifluoroethylene monomer, 10.44% of methyl isobutyl ketone, 24.38% of dimethylbenzene, 0.832% of azodiisobutyronitrile, 1.024% of undecylenic acid, 2.894% of allyl alcohol and 21.87% of vinyl acetate, wherein, CTFE is the abbreviation for the chlorotrifluoroethylene monomer, and MIBK is the abbreviation for methyl isobutyl ketone. The synthesis process comprises the following steps: preparing, adding raw materials to a polymerization kettle, vacuumizing the polymerization kettle, adding the trifluorochloroethylene chlorotrifluoroethylene monomer raw material to the polymerization kettle, stirring and heating, and finally discharging the fluorocarbon resin. The fluorocarbon resin has durability, weatherability and chemical resistance, and shows special surface properties such as remarkable non-stick property, low surface tension, low friction property, water repellency, oil repellency and the like; and various coatings prepared by the fluorocarbon resin have outstanding high adhesive force and outstanding environmental aging resistance.

Description

technical field [0001] The invention relates to a synthesis process of fluorocarbon resin, in particular to a solvent-type fluorocarbon resin. Background technique [0002] Chinese patent "ultra-low surface energy type fluorocarbon resin", the patent number is 03112337.6, discloses a low surface energy type fluorocarbon resin, which is to introduce organosilicone ester during the polymerization of fluorocarbon resin, so that the fluorocarbon resin can It has a lower surface tension when forming a film, which further improves the self-cleaning property of the paint film. The method and formula of this patent mainly solve the surface tension of fluorocarbon resin in application and improve the self-cleaning property. [0003] At present, people still produce fluorocarbon resin through traditional synthesis process polymerization. The traditional synthesis process has a long production cycle and generally takes 72 hours to complete; after the polymerization reaction, the produc...

Claims

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Application Information

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IPC IPC(8): C08F214/24C08F220/04C08F216/08C08F218/08C08F2/01C09D127/12
Inventor 周法现
Owner 徐州中研科技工业有限公司
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