Method for preparing p-CoO/n-CdS compound semiconductor photocatalyst
A compound semiconductor and photocatalyst technology, which is applied in the field of photocatalytic materials, can solve problems that have not been reported in the literature, and achieve the effects of reducing photocorrosion, improving photocatalytic efficiency, and increasing specific surface area
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Embodiment 1
[0035] Preparation of CdS solid powder product:
[0036] Anhydrous ammonium sulfate: 24%
[0037] Anhydrous cadmium sulfate: 11%
[0038] Thiourea: 5%
[0039] Deionized water: 60%
[0040] The preparation of CdS solid powder product is according to anhydrous ammonium sulfate: anhydrous cadmium sulfate: thiourea: the ratio by weight of deionized water is 24%: 11%: 5%: 60%, anhydrous ammonium sulfate, anhydrous sulfuric acid Mix cadmium, thiourea and deionized water, pre-react for 0.5h in a microwave reactor with a power of 500W, and then react at a frequency of 53KH Z , Under ultrasonic dispersion with a power of 350W, react at 80°C for 10h to obtain a reaction product; the reaction product is filtered to obtain a yellow CdS primary solid powder cake; the CdS primary solid powder cake is added to deionized water 5 times its weight, washed with deionized water, and ultrasonically Disperse for 1 hour and filter, and repeat the above operation three times to obtain CdS second...
Embodiment 2
[0048] Preparation of CdS solid powder product:
[0049] Anhydrous Ammonium Chloride: 34.5%
[0050] Cadmium nitrate tetrahydrate: 15.4%
[0051] Thiourea: 7.1%
[0052] Deionized water: 50%
[0053] The preparation of CdS solid powder product is according to anhydrous ammonium chloride: cadmium nitrate tetrahydrate: thiourea: the ratio by weight of deionized water is 34.5%: 15.4%: 7.1%: 50%, anhydrous ammonium chloride, tetrahydrate Water cadmium nitrate, thiourea, and deionized water are mixed, firstly reacted in a microwave reactor with a power of 300W for 1h, and then heated at a frequency of 53KH Z , Under ultrasonic dispersion with a power of 250W, react at 90°C for 5 hours to obtain a reaction product; the reaction product is filtered to obtain a yellow CdS primary solid powder cake; the CdS primary solid powder cake is added to deionized water 5 times its weight, washed with deionized water, and ultrasonically Disperse for 1 hour and filter, and repeat the above oper...
Embodiment 3
[0061] Preparation of CdS solid powder product:
[0062] Trimethylamine Sulfate: 12%
[0063] Anhydrous cadmium chloride: 12.8%
[0064] Thiourea: 10.2%
[0065] Deionized water: 65%
[0066] The preparation of CdS solid powder product is according to trimethylamine sulfate: anhydrous cadmium chloride: thiourea: the ratio by weight of deionized water is 12%: 12.8%: 10.2%: 65%, trimethylamine sulfate, anhydrous Mix cadmium chloride, thiourea and deionized water, pre-react for 0.5h in a microwave reactor with a power of 600W, and then react at a frequency of 53KH Z , Under ultrasonic dispersion with a power of 200W, react at 85°C for 4h to obtain a reaction product; the reaction product is filtered to obtain a yellow CdS primary solid powder cake; the CdS primary solid powder cake is added to deionized water 5 times its weight, washed with deionized water, and ultrasonically Disperse for 1 hour and filter, and repeat the above operation three times to get CdS secondary solid...
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