Method for quickly detecting doping of benzodiazepine compound in food, medicine or health-care product
A medium benzodiazepine and detection method technology is applied in the field of rapid detection doped with benzodiazepines, and can solve the problem that the specific combination of a gold-labeled reagent and a test substance cannot be realized, and the colloidal gold immunity cannot be fully exerted. The advantages of chromatographic detection and the unknown amount of illegally adulterated benzodiazepines have achieved the effect of rapid screening, fast detection and low cost
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Embodiment 1
[0044] Embodiment 1 Yimengxiang Melatonin Capsules
[0045] The Yimengxiang Melatonin Capsules of this embodiment is a health food, and the dosage form is a capsule. First, prepare the test equipment:
[0046] Container with stopper (10ml), disposable filter, small glass bottle, benzodiazepine colloidal gold test paper.
[0047] The detection method of the present embodiment, its specific steps are as follows:
[0048] (1) Take 1 Yimengxiang melatonin capsule, open the capsule, pour the contents into a stoppered container, add 1ml of absolute ethanol, shake for 10 seconds, add water to make up the total volume to 10ml, put the stoppered container After the liquid in the filter is filtered, the filtrate is collected;
[0049] (2) Put the filtrate collected above into a small glass bottle, insert the benzodiazepine colloidal gold detection test paper into it, take out the test paper after 2 minutes, place it flat, and observe the color changes of the reaction line and the cont...
Embodiment 2 7
[0052] Example 2 Aescin Tablets
[0053] The Qiye Shen'an tablet of this embodiment is a Chinese patent medicine, and the dosage form is a tablet. First, prepare the test equipment:
[0054] Container with stopper (10ml), disposable filter, small glass bottle, benzodiazepine colloidal gold test paper, paper disc, pestle.
[0055] The detection method of the present embodiment, its specific steps are as follows:
[0056] (1) Take 1 Aescin tablet, put it on a piece of paper, grind it finely with a pestle, pour it into a container with a stopper, add 1ml of absolute ethanol, shake for 10 seconds, add water to make up the total volume to 10ml, and put the stopper After the liquid in the container is filtered, the filtrate is collected;
[0057] (2) Put the filtrate collected above into a small glass bottle, insert the benzodiazepine colloidal gold detection test paper into it, take out the test paper after 2 minutes, place it flat, and observe the color changes of the reaction l...
Embodiment 3 3
[0060] Embodiment 3 Sanshengbao sleeps in peace (sleeping tablet)
[0061] Sansheng Baoshui Er'an (Sleeping tablets) of the present embodiment is a health food, and its dosage form is a tablet. At first prepare the test equipment:
[0062] Container with stopper (10ml), disposable filter, small glass bottle, benzodiazepine colloidal gold test paper, paper disc, pestle.
[0063] The detection method of the present embodiment, its specific steps are as follows:
[0064] (1) Take 1 tablet of Sanshengbao Sleeper’an, put it on a piece of paper, grind it finely with a pestle, pour it into a stoppered container, add 1ml of absolute ethanol, shake for 10 seconds, add water to make up the total volume to 10ml, After filtering the liquid in the stoppered container, collect the filtrate;
[0065] (2) Put the filtrate collected above in a small glass bottle, put the filtrate in a small glass bottle, insert the benzodiazepine colloidal gold detection test paper into it, take out the test...
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