Substrate with surface-enhanced Raman scattering activity and preparation method thereof
A surface-enhanced Raman and active substrate technology, applied in Raman scattering, material excitation analysis, etc., can solve problems such as poor reusability, complicated preparation methods, and shedding of SERS active substances, and achieve the effect of improving the reusability rate
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Embodiment 1
[0037] The preparation method of active substrate with surface-enhanced Raman scattering is divided into two steps:
[0038] (1) Hydroxylation treatment and amination treatment of glass substrates
[0039] Mix concentrated sulfuric acid with a mass fraction of 98% and hydrogen peroxide with a mass fraction of 30% at a volume ratio of 7:3, and the substrate is oxidized and cleaned at 90°C for 40 minutes in the mixed solution, rinsed with distilled water, and dried with nitrogen; The hydroxylated substrate was placed in an acetone solution of APTMS with a concentration of 20mmol for assembly for 4h.
[0040] (2) Preparation of surface-enhanced Raman scattering (SERS) active substrates
[0041] The "oscillating method" was used to prepare silica microspheres, using ethanol as a solvent and ammonia as a catalyst to catalyze the hydrolysis of ethyl orthosilicate to obtain particles with a particle size of 200-250nm; then add 20mg of silica to a 60mL anhydrous Add 200 μL of APTMS to...
Embodiment 2
[0043] (1) Carry out hydroxylation treatment and amination treatment to the glass substrate first
[0044] Mix concentrated sulfuric acid with a mass fraction of 98% and hydrogen peroxide with a mass fraction of 30% at a volume ratio of 7:3. The substrate is oxidized and cleaned at 90°C for 60 minutes in the mixed solution, rinsed with distilled water, and dried with nitrogen; The hydroxylated substrate was placed in a n-hexane solution of APTMS with a concentration of 30 mmol and assembled for 3 h.
[0045] (2) Preparation of surface-enhanced Raman scattering (SERS) active substrate
[0046] Silica microspheres were prepared by "vibration method", using isopropanol as solvent and ammonia water as catalyst to catalyze the hydrolysis of ethyl orthosilicate to obtain particles with a particle size of 200-250nm; then add 50mg of silica to a 100mL container Add 400 μL APTES to the Erlenmeyer flask of absolute ethanol, and place it in a shaker for 24 hours to obtain SiO 2 -NH 2 ...
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