Method for producing open tubular electrophoresis column coating with nano titanic oxide and uses thereof
A nano-titanium dioxide, electrophoresis column technology, applied in chemical instruments and methods, separation methods, other chemical processes, etc., can solve the problems of uncontrollable reaction rate, uneven mixing of reactants, high cost of metal alkoxides, and reduce non-specificity. The effect of adsorption, good chemical bonding strength and simple and easy preparation method
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0038] Preparation of open-tube electrophoresis column: Stir 1ml of absolute ethanol, 0.34g of tetrabutyl titanate, and 0.2875g of polyethylene oxide-polypropylene oxide-polyethylene oxide, and pass N2 to remove dissolved oxygen. Add HCl solution to adjust the pH to 1-2, heat the reaction kettle to 130°C, and react for 12 hours. Finally, rinse with ethanol to remove the porogen. figure 1 Electron micrograph of the combined surface of SiO2-TiO2 coated nano-titanium dioxide open-tube electrophoresis column.
Embodiment 2
[0040] Preparation of open-tube electrophoresis column: Stir 1ml of absolute ethanol, 0.34g of tetrabutyl titanate, and 0.63g of polyoxyethylene-polyoxypropylene-polyoxyethylene block copolymer evenly, and pass N 2 After removing dissolved oxygen, add HCl solution to adjust the pH to 1-2, heat the reactor to 150°C, and react for 11 hours. Finally, rinse with ethanol to remove the porogen. figure 2 Enrichment mass spectrum of β-casein hydrolysis product for titanium dioxide open-tube column.
Embodiment 3
[0042]Preparation of open-tube electrophoresis column: Stir 1ml of absolute ethanol, 0.34g of tetrabutyl titanate, 0.2875g of polyethylene oxide-polypropylene oxide-polyethylene oxide, and pass N 2 After removing the dissolved oxygen, add HCl solution to adjust the pH to 1-2, heat the reactor to 130°C, and react for 12 hours. Finally, rinse with ethanol to remove the porogen. image 3 The mass spectrum of α-casein (5picomoles) enzymatic hydrolysis product was enriched for titanium dioxide open-tube column.
PUM
Property | Measurement | Unit |
---|---|---|
The inside diameter of | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com