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U shape tubular isothermal low-temperature methanol synthesis tower

A methanol synthesis tower, isothermal technology, applied in the preparation of hydroxyl compounds, organic compounds, chemical instruments and methods, etc., can solve the problems of cold pipe and ring pipe weld cracking, affecting the uniform distribution of air flow, affecting production, etc. Achieve the effects of reduced material requirements, stable operation, and convenient loading and unloading

Inactive Publication Date: 2006-07-12
ZHEJIANG UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, for the fixing of the two ends of the descending cold pipe in the U-shaped cold pipe, there is a certain thermal stress, which is likely to cause cracking at the weld between the cold pipe and the ring pipe, seriously affecting production.
[0007] In addition, with the expansion of production capacity, the diameter of the synthesis tower has increased to 2-4m, and the absence of a gas distributor at the inlet of the tower will also affect the uniform distribution of the gas flow, thereby affecting the reaction.

Method used

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  • U shape tubular isothermal low-temperature methanol synthesis tower

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Embodiment Construction

[0027] The present invention will be further described below in conjunction with the accompanying drawings.

[0028] refer to figure 1 , the synthesis tower of the present invention is made up of two large parts of outer cylinder and internal parts, and outer cylinder comprises: gas distributor (1), upper sealing head (2), cylinder body (6), positioning ring (9), lower sealing head ( 13); the internal parts include: clapboard (4), cold tube liner (7), support ring (8), wherein cold tube liner (7) is composed of air induction tube (3), ring tube (5), descending cold tube ( 10), the ascending cold pipe (11) is assembled and welded, supported on the positioning ring (9) welded on the inner wall of the outer cylinder by the support ring (8), and the catalyst (12) is filled outside the cold pipe. The top of the last head (2) is welded with the air intake pipe a, the bottom of the lower head (13) is welded with the outlet pipe b, the top of the head is welded with the baffle plate ...

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Abstract

The invention relates to a new U-shaped isothermal low-pressure methanol converter, comprising a outer cylinder, and inner elements, wherein, said outer cylinder comprises a upper closure head, a cylinder body, a positioning ring, and a lower closure head; and said inner elements comprises a separation plate, a cold gallbladder, and a support ring, while said upper closure head has a charging pipe; said lower closure head has a discharging pipe; the air guiding pipe of cold gallbladder is sealed on the separation plate with stuffing and catalyst is arranged outside said cold gallbladder; the cold gallbladder pipe is in multiple rings U-shaped and via support ring supported on the positioning ring welded on the inner wall of outer cylinder to hang and support cold gallbladder; said outer cylinder also comprises a new air distributor inside the upper closure head to connect the charging pipe. The invention provides a new U-shaped isothermal low-pressure methanol converter with uniformly distributed charged air, high synthesizing efficiency, simple structure and lower producing cost, which can apply large methanol synthesizing device.

Description

(1) Technical field [0001] The invention belongs to a cold tube type gas-solid phase reactor, which is especially suitable for low-pressure methanol synthesis, and can also be used for the synthesis reaction of ammonia and dimethyl ether. (2) Background technology [0002] Low-pressure methanol synthesis, due to low synthesis pressure and low overall energy consumption, low-pressure synthesis is generally used for large-scale production of methanol at home and abroad, and the synthesis pressure is 5-10 MPa. Copper-based catalyst is used, the reaction temperature is 200-280°C, and the space velocity is 6000-10000h -1 . [0003] The methanol synthesis reaction has a large heat release, while the methanol catalyst has poor heat resistance and a narrow range of active temperatures. The conversion rate of synthetic methanol under low pressure is higher than that under low pressure. Catalyst loading capacity is large. Therefore, the low-pressure methanol synthesis tower not on...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/02C07C29/152C07C31/04
Inventor 刘华彦陈运根
Owner ZHEJIANG UNIV OF TECH
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