Process for fabricating circuit assemblies using electrodepositable dielectric coating compositions
A composition and electrodeposition technology, applied in electrophoretic coatings, printed circuit parts, circuits, etc., can solve problems such as insufficient electrical insulation performance
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Embodiment A
[0096] This example describes the preparation of the electrodepositable coating composition used in Example 1 below. These resin binders were prepared from the following ingredients as described below. The listed values represent parts by weight (unit: gram).
[0097] components
Example A
crosslinking agent 1
1882
Diethylene glycol monobutyl ether formal
108.78
EPON®828 2
755.30
694.90
TETRONIC 150R1 3
0.33
51.55
Aminopropyldiethanolamine
113.2
remove distillate
(67.66)
45.17
deionization
2714
1.70
Resin intermediate 5
244.7
rosin 5
27.49
Deionized water
2875
[0098] components
parts by weight (g)
92.0
456.0
Polyol a
739.5
methyl isobu...
Embodiment 1
[0112] 1 Catalyst slurry, purchased from PPG Industries, Inc.
[0113] The ingredients listed above are combined and mixed with gentle agitation. The composition was ultrafiltered 50% and reconstituted with deionized water.
[0114] Preparation of circuitized substrates
[0115] An INVAR metal perforated monolayer (50 microns thick, supplied by Buckbee-Mears, a division of BMC Industries, Inc.) containing 200 micron diameter holes spaced 500 microns apart (center to center) in a square grid arrangement was cleaned and microetched etch to remove unwanted dirt, oil and oxides. The pre-cleaned perforated substrate was then electroplated to provide a copper metal layer with a thickness of 9 microns.
[0116] The electrodepositable coating composition of Example 1 above was electrophoretically applied to the plated substrate in an electrodeposition bath at a temperature of 105°F (41°C) at 90 volts for 2 minutes. The electrocoated substrate was rinsed with deionized wate...
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