Method for producing high-efficiency washing soap powder by using sewer oil or swill oil
A technology for swill oil and waste oil, which is applied in chemical instruments and methods, detergent powder/sheet/sheet, detergent composition, etc., to achieve the effects of solving losses, reducing environmental pollution and major social value
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Embodiment 1
[0028] (1) Add 500 kg of waste oil into a 1500 liter enamel reaction tank, then add 400 kg of clear water, heat up to 60°C, stir for 1 hour, dissolve and mix;
[0029] (2) add 40 kilograms of NaCl in above-mentioned retort, stir and simultaneously insulate 30 minutes, leave standstill then, oil layer, water layer appear;
[0030] (3) Separating the oil layer and filtering it with a 30-purpose filter screen to obtain the filtrate;
[0031] (4) Weigh 300 kg of filtrate, put it into a 1000-liter reaction tank, add 30 kg of activated carbon and activated clay mixture in a ratio of 1:8, heat up to 140 ° C, stir for 1.5 hours, filter with a 60-mesh filter screen, and obtain the filtrate ;
[0032] (5) take step (4) and make 400 kilograms of filtrates, add 180 kilograms of clear water, volume concentration is 50 kilograms of industrial grade sulfuric acid of 76%, volume concentration is 3 kilograms of alkylbenzenesulfonic acids of 1%, stir and be warming up to 110°C, react for 12 h...
Embodiment 2
[0039] (1) Add 500 kg of swill oil into a 1500 liter enamel reaction tank, then add 350 kg of clear water, heat up to 75°C, stir for 1 hour, dissolve and mix;
[0040] (2) add 35 kilograms of NaCl in above-mentioned reaction tank, stir and simultaneously insulate for 30 minutes, leave standstill then, oil layer, water layer occur;
[0041] (3) Separating the oil layer and filtering it with a 30-purpose filter screen to obtain the filtrate;
[0042] (4) Weigh 350 kg of filtrate, put it into a 1000-liter reaction tank, add 40 kg of activated carbon and activated clay mixture in a ratio of 1:7, heat up to 150 ° C, stir for 2 hours, filter with a 70-mesh filter screen, and obtain the filtrate ;
[0043] (5) Take by weighing 300 kilograms of filtrate obtained in step (4), add 200 kilograms of clear water, 60 kilograms of sulfuric acid with a volume concentration of 50%, and 4 kilograms of alkylbenzenesulfonic acids with a volume concentration of 1%, stir and be heated to 120° C. ...
Embodiment 3
[0050] Weigh raw materials according to the following weight ratio:
[0051] 100 parts of waste oil, 12 parts of 50% dilute sulfuric acid, 20 parts of caustic soda, 4 parts of a mixture of activated carbon and activated clay with a weight ratio of 1:6, 0.8 parts of alkylbenzenesulfonic acid, 8 parts of sodium chloride, and 16 parts of high-efficiency additives , 12 parts of a mixture of sodium sulfate, sodium carbonate and sodium silicate.
[0052] Preparation method: Add 100 parts of waste oil into an enamel reaction tank, add 100 parts of clear water, raise the temperature to 60°C, stir for one hour, add 7 parts of sodium chloride, stir for 0.5 hours, let the layers stand still, release the lower layer of water, and then add 4 parts The mixture of activated carbon and activated clay is heated to 150°C, stirred for one hour, and centrifugally filtered with a 50-mesh filter. 0.8 parts of benzenesulfonic acid, heated up to 120°C, reacted for 10 hours, separated into layers, wa...
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