Methyl-amino-ivermectin water suspension nano capsule prepn and its preparing method
A technology of emamectin and nanocapsules, applied in botany equipment and methods, biocides, animal repellents, etc., can solve problems such as waste of resources, waste of decomposition, pesticide residues, etc., and achieve ecological benefits Effects of environment, improved utilization, and improved stability
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Embodiment 1
[0056] Dissolve 0.1g of ammonium persulfate in 20g of water (divided into two parts according to 4:1), and set aside; dissolve 0.5g of emamectin in the mixed monomer of 7g of styrene, 8g of butyl acrylate, and 0.2g of acrylic acid In; 6gOP-40, 1g sodium lauryl sulfate are dissolved in 50g 2% polyvinyl alcohol aqueous solution, put into a container with agitation, under stirring, add the mixing single that emamectin is dissolved body, dispersed into an emulsion, and placed in a reaction vessel. Heat to keep the temperature at 70±2°C, add the first part of initiator, react for 6 hours, keep warm for 1 hour, and prepare the seed emulsion; add 1.5g of styrene, 1.5g of butyl acrylate, 2g of toluene diisocyanate mixed monomer and Add the second initiator dropwise for 1 hour, keep warm for 2 hours, cool down; add additives, and discharge. The content of emamectin in the product is 0.5%.
Embodiment 2
[0058] Dissolve 0.1g of potassium persulfate in 10g of water (divided into two parts according to 4:1), 1g of acrylamide is dissolved in 10g of water for use; 1g of emamectin is dissolved in 4g of ethyl acrylate and 7g of butyl acrylate In the mixed monomer; dissolve 5g OP-40, 4g sodium lauryl sulfate, and 4g sodium polymethacrylate in 60g water, put them into a stirring container, and add the dissolved Avermectin The mixed monomers of the element are dispersed into an emulsion and put into the reaction vessel. Heat and keep the temperature at 70±2°C, add the first initiator and acrylamide aqueous solution, react for 6 hours, keep warm for 1 hour, and prepare the seed emulsion; add 1g ethyl acrylate, 1g butyl acrylate, 2g 4,4' - diphenylmethane diisocyanate mixed monomer, dropwise for 1 hour, keep warm for 2 hours, cool down; add additives, discharge. The content of emamectin in the product is 0.9%.
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