Process for preparing nano zinc oxide material
A nano-zinc oxide and sodium hydroxide technology, applied in the direction of zinc oxide/zinc hydroxide, etc., can solve the problems of difficult control of reaction conditions, fast crystal nucleus growth process, insufficient ball milling time, etc., and achieve controllable reaction conditions and simple equipment , the effect of high yield
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[0008] Below in conjunction with embodiment the present invention will be further described,
[0009] According to the chemical composition sodium hydroxide NaOH: zinc nitrate Zn (NO 3 ) 2 = 4.8:1.8, mix at room temperature, grind and mix for 40 minutes, heat to 380°C for thermal decomposition, and get zinc oxide NZnONO 3 , sodium nitrate NaNO 3 The mixed solution was cooled to 70° C., washed with 5% deionized water, precipitated and filtered to obtain a filter cake containing ZnO. Cool the filter cake to 35°C, add 10% ethanol to wash with alcohol for 5 hours, and filter under normal pressure, add an appropriate amount of CaCO to the filtrate 3 , The alcohol washed cake was dried at 45°C for 2 hours, and then calcined at 750°C to obtain nano-zinc oxide powder material.
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