Coated glass with dual function of cutting-off ultraviolet ray / reflecting infrared ray and preparation method thereof

A coated glass, dual-function technology, applied in the field of glass and its preparation, can solve the problems of difficult control of cerium ion addition, complicated process, etc., and achieve the effects of preventing heat transfer from glass, simple and flexible process, and broad prospects.

Inactive Publication Date: 2006-11-29
WUHAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The problem is that although cerium ions absorb ultraviolet rays, they still partially transmit glass; in addition, glass is prepared by melting to absorb ultraviolet rays, the process is complicated, and the amount of cerium ions added is not easy to control

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0016] A method for preparing a coating glass with dual functions of cutting off ultraviolet rays / reflecting infrared rays, comprising the following steps:

[0017] 1). Firstly, after cleaning and drying the glass substrate to be coated, carry out pre-vacuum transition;

[0018] 2). Then the magnetron sputtering method is used to coat the film layer: (1). Two kinds of targets are prepared: the titanium oxide-cerium oxide target is composed of titanium oxide and cerium oxide, and the cerium oxide and titanium oxide in the target The mass ratio is 1 / 3; the transparent wide bandgap semiconductor oxide target is In 2 o 3 and Sn targets, In 2 o 3 : The mass ratio of Sn is 50.0%: 50.0%;

[0019] (2).Magnetron sputtering coating: Carry out magnetron sputtering coating on the glass substrate in pure argon atmosphere, the sputtering pressure is 0.4Pa; The inner film is sputtered and the thickness of the film is 210nm. On this basis, In 2 o 3 Continue coating with Sn target to ge...

example 2

[0023] A method for preparing a coating glass with dual functions of cutting off ultraviolet rays / reflecting infrared rays, comprising the following steps:

[0024] 1). Firstly, after cleaning and drying the glass substrate to be coated, carry out pre-vacuum transition;

[0025] 2). Then the magnetron sputtering method is used to coat the film layer: (1). Two kinds of targets are prepared: the titanium oxide-cerium oxide target is composed of titanium oxide and cerium oxide, and the cerium oxide and titanium oxide in the target The mass ratio is 1 / 3; the transparent wide bandgap semiconductor oxide target is In 2 o 3 and Sn targets, In 2 o 3 : The mass ratio of Sn is 99.0:1.0;

[0026] (2). Magnetron sputtering coating: Carry out magnetron sputtering coating on the glass substrate in the oxygen-argon mixed gas atmosphere, the sputtering pressure is 0.4Pa, and the mass ratio of the argon-oxygen mixed gas during sputtering is oxygen: argon =1:20; Firstly, the inner layer fi...

example 3

[0030] A method for preparing a coating glass with dual functions of cutting off ultraviolet rays / reflecting infrared rays, comprising the following steps:

[0031] 1). Firstly, after cleaning and drying the glass substrate to be coated, carry out pre-vacuum transition;

[0032] 2). Then the magnetron sputtering method is used to coat the film layer: (1). Two kinds of targets are prepared: the titanium oxide-cerium oxide target is composed of titanium oxide and cerium oxide, and the cerium oxide and titanium oxide in the target The mass ratio of ZnO: Al is 3 / 2; the transparent wide bandgap semiconductor oxide target material is ZnO and Al target material, and among the ZnO and Al target material, the mass ratio of ZnO:Al is 85.0%%:15.0%;

[0033] (2). Magnetron sputtering coating: Carry out magnetron sputtering coating on the glass substrate in the oxygen-argon mixed gas atmosphere, the sputtering pressure is 0.4Pa, and the mass ratio of the argon-oxygen mixed gas during sputt...

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Abstract

The invention belongs to building glass material, automobile using glass material and light fitting glass technique field. The coated glass with dual function of ultraviolet ray cutting off and infrared ray reflecting is includes substrate glass. Its features are that the substrate glass is coated infrared ray reflecting film and ultraviolet ray cutting off film. The ultraviolet ray cutting off film is titanium oxide- cerium oxide film, and both of their mass ratios are from ten percent to ninety percent. The infrared ray reflecting film is transparent bandwidth gap semiconductor oxide film, and it is one of the three as the following In2O3: Sn film, SnO2: Sb film, ZnO: AL film. And their mass ratios respectively are from 50.0percent to 99.0 percent to from 1.0 percent to 50.0 percent, from 80.0 percent to 99.9 percent to from 0.1 percent to 20.0 percent, and from 85.0 percent to 99.9 percent to from 0.1 percent to 15.0 percent. The invention that the cut-off ratio of the ultraviolet ray of is high, not influences the visible light transmittance, and has the function of saving energy. Its preparation method is simple.

Description

technical field [0001] The invention belongs to the technical field of architectural glass materials, automotive glass materials and lighting lamp glass, and in particular relates to a glass with a double-functional film layer for cutting ultraviolet rays and reflecting infrared rays coated on a glass substrate by a magnetron sputtering method and a preparation method thereof. Background technique [0002] Ultraviolet rays will age high molecular organic matter. In some special occasions, it is necessary to prevent ultraviolet rays from entering or exiting the glass. Substances in living rooms, museums, and cars, such as paper, fabrics, and some precious cultural relics, will age and deteriorate under ultraviolet radiation. [0003] At present, the method of preparing UV-blocking glass is to add cerium ions, Ce +3 Acting as a strong hole-trapping center, Ce +4 It plays a strong role in capturing electrons, so that the electrons and holes generated by the irradiation are c...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C4/00C03C4/08C03C17/34C03C17/22
Inventor 赵青南倪佳苗赵修建
Owner WUHAN UNIV OF TECH
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