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Low-temperature co-fired ceramic material for filter as well as preparation method and application of low-temperature co-fired ceramic material

A low-temperature co-fired ceramic and filter technology, which is applied in the field of low-temperature co-fired ceramic material preparation, can solve the problems of high sintering temperature, inability to achieve low-cost, low-energy-consumption industrial applications, and achieves improved low-temperature sintering performance and obvious cost advantages. and integrated advantages, the effect of improving the quality factor

Active Publication Date: 2022-07-29
SHANDONG SINOCERA FUNCTIONAL MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the sintering temperature of this material system is relatively high (>1200°C), making it impossible to achieve low-cost, low-energy industrial applications

Method used

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  • Low-temperature co-fired ceramic material for filter as well as preparation method and application of low-temperature co-fired ceramic material
  • Low-temperature co-fired ceramic material for filter as well as preparation method and application of low-temperature co-fired ceramic material
  • Low-temperature co-fired ceramic material for filter as well as preparation method and application of low-temperature co-fired ceramic material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0060] The low-temperature co-fired ceramic material described in this embodiment, in terms of the total amount of its preparation raw materials, includes the following components in mass content:

[0061] BaTi 4 O 9 60wt%;

[0062] MgTiO 3 20wt%;

[0063] Low melting point glass powder 20wt%;

[0064] Wherein, the low melting point glass powder includes the following components by weight:

[0065]

[0066] The preparation method of the low-temperature co-fired ceramic material described in this embodiment includes the following steps:

[0067] According to the selected mass content ratio, take the ZnO, SiO 2 , BaCO 3 , B 2 O 3 , Li 2 O, Al 2 O 3 Mix evenly, and carry out melting treatment at 1300 °C. After the molten glass is cooled, it is pulverized by a roller mill. After pulverization, it is ground with a dry ball mill and a jet mill. The particle size after grinding is required to be less than 2 μm. Need low melting point glass powder, spare;

[0068] T...

Embodiment 2

[0070] The low-temperature co-fired ceramic material described in this embodiment, in terms of the total amount of its preparation raw materials, includes the following components in mass content:

[0071] BaTi 4 O 9 65wt%;

[0072] MgTiO 3 15wt%;

[0073] Low melting point glass powder 20wt%;

[0074] Wherein, the low melting point glass powder includes the following components by weight:

[0075]

[0076] The preparation method of the low-temperature co-fired ceramic material described in this embodiment includes the following steps:

[0077] According to the selected mass content ratio, take the ZnO, SiO 2 , BaCO 3 , B 2 O 3 , Li 2 O, Al 2 O 3 Mix evenly, and carry out melting treatment at 1300 °C. After the molten glass is cooled, it is pulverized by a roller mill. After pulverization, it is ground with a dry ball mill and a jet mill. The particle size after grinding is required to be less than 2 μm. Need low melting point glass powder, spare;

[0078] T...

Embodiment 3

[0080] The low-temperature co-fired ceramic material described in this embodiment, in terms of the total amount of its preparation raw materials, includes the following components in mass content:

[0081] BaTi 4 O 9 65wt%;

[0082] MgTiO 3 10wt%;

[0083] Low melting point glass powder 25wt%;

[0084] Wherein, the low melting point glass powder includes the following components by weight:

[0085]

[0086] The preparation method of the low-temperature co-fired ceramic material described in this embodiment includes the following steps:

[0087] According to the selected mass content ratio, take the ZnO, SiO 2 , BaCO 3 , B 2 O 3 , Li 2 O, Al 2 O 3 Mix evenly, and carry out melting treatment at 1300 °C. After the molten glass is cooled, it is pulverized by a roller mill. After pulverization, it is ground with a dry ball mill and a jet mill. The particle size after grinding is required to be less than 2 μm. Need low melting point glass powder, spare;

[0088] T...

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Abstract

The invention belongs to the technical field of low-temperature co-fired ceramic materials, particularly relates to a ceramic material with high ceramic forming compactness, medium dielectric constant, low dielectric loss and near-zero resonant frequency coefficient, and further discloses a preparation method of the low-temperature co-fired ceramic material. According to the low-temperature co-fired ceramic material disclosed by the invention, BaTi4O9, MgTiO3 and low-melting-point glass are taken as raw materials, and after the raw materials are subjected to composite sintering, the stability of the low-temperature co-fired ceramic material along with temperature change becomes good, the quality factor of the material is relatively high, the dielectric constant is 19-25, and the use requirements of sub6GHz microwave devices are met; and the sintering temperature of the material is reduced from 1250 DEG C to 850-900 DEG C, so that the low-temperature sintering performance of the material is greatly improved, and industrial production is facilitated.

Description

technical field [0001] The invention belongs to the technical field of low-temperature co-fired ceramic materials, in particular to a ceramic material with high ceramic compactness, medium dielectric constant, low dielectric loss and near-zero resonance frequency coefficient, which can be used for preparing dielectric filters in the field of electronic communications , dielectric antenna and other components, and further discloses the preparation method of the low-temperature co-fired ceramic material. Background technique [0002] In recent years, with the rapid development of emerging communication technologies such as 5G, the number of 5G base stations has greatly increased, and the demand for filters as the core components of the radio frequency front-end of base stations has skyrocketed. At present, there are three main types of common filters, including metal coaxial cavity filters, ceramic dielectric resonant filters, and ceramic dielectric filters. Among them, ceram...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/468C04B35/622C04B35/63
CPCC04B35/468C04B35/622C04B35/6303C04B2235/3236C04B2235/3203C04B2235/3284C04B2235/3409C04B2235/3418C04B2235/3217C04B2235/5427C04B2235/77
Inventor 宋锡滨刘振锋艾辽东奚洪亮张忠楠闫鑫升
Owner SHANDONG SINOCERA FUNCTIONAL MATERIAL CO LTD
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