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Reinforcing method of continuous carbon fiber toughened ceramic matrix composite material

A technology of toughening ceramics and composite materials, applied in the field of ceramic composite materials, can solve problems such as development time, cost waste, shedding failure, repair failure, etc., achieve a wide range of use environments, improve repair reliability, and improve performance.

Active Publication Date: 2022-02-08
AEROSPACE INST OF ADVANCED MATERIALS & PROCESSING TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When continuous carbon fiber toughened silicon carbide ceramic matrix composites are used in high-temperature airflow and particle erosion environments, the components will suffer from wear and oxidation damage, resulting in damage to the components that cannot continue to be used
During the service of composite components, usually only the parts with the most severe local service conditions (such as the highest local temperature, a large number of local particle erosion) have serious defects, which makes the components unusable; even under extreme conditions, the components are severely damaged locally Can cause composite components to fail to meet harsh service conditions
Great waste of development time and cost
[0003] CN106986664A discloses a method of repeatedly impregnating and cracking polycarbosilane using carbon cloth and SiC micropowder to C f / The method of repairing the damaged area of ​​SiC composite material, this method only repairs the damaged component, and the repaired area is close to the mechanical properties of the overall component composite material, which cannot effectively prevent the repaired area from being damaged and failed again. At the same time, the repaired area and the material body The lack of physical connection between the patches causes the patch to fall off easily in the heat environment during use, resulting in repair failure; CN104150958A uses carbon fiber prepreg cloth to fill the defective part, then molds and solidifies, coats the slurry, and then pyrolyzes and deposits SiC coating The method of repairing ceramic matrix composites, but this method also lacks physical connection, and it is easy to fall off and fail in the heat environment

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] This embodiment provides a continuous carbon fiber reinforced ceramic matrix composite reinforcement method, the specific process is as follows:

[0042] 1. Use ethanol to clean the new acupuncture structure C / SiC component body, including the component body and connection parts.

[0043] 2. Design the needle-punched structure C / SiC-ZrC patch material as a trapezoidal hexahedron matching the groove of the component, and the component and the patch material are connected by threads to complete the physical connection.

[0044] 3. Use high-temperature adhesive to coat all connecting parts and surfaces. The adhesive contains Si, C, and O, which can meet the requirements of 1200°C.

[0045] 4. Install patch.

[0046] 5. Use the PIP process for online connection, the solution used is the SiBCN precursor solution, repeat the PIP process twice to complete the reinforcement.

[0047] The continuous carbon fiber toughened ceramic matrix composite member (referred to as sample ...

Embodiment 2

[0051] This embodiment provides a continuous carbon fiber reinforced ceramic matrix composite reinforcement method, the specific process is as follows:

[0052] 1. Use acetone to clean the body of the damaged component needle-punched C / SiC-ZrC component, including the connection part.

[0053] 2. Flare the damaged part into a circular shape, and the patch material is punctured C / SiC-ZrC-HfC-TaC composite material, which is designed to be cylindrical, and the patch material and the component body are connected by threads.

[0054] 3. Use high-temperature adhesive to coat all connecting parts and surfaces. The adhesive contains Si, C, and O, which can meet the requirements of 1200°C.

[0055] 4. Install patch.

[0056] 5. Use PIP process for online connection, use PCS solution for connection, repeat PIP process 3 times.

[0057] 6. Manually polish the surface to remove excess such as steps.

[0058] 7. The SiC coating is prepared by the overall CVD process to complete the rei...

Embodiment 3

[0063] This embodiment provides a continuous carbon fiber reinforced ceramic matrix composite reinforcement method, the specific process is as follows:

[0064] 1. For the new acupuncture structure C / SiC-ZrB 2 The component body is cleaned with ethanol, including the joints.

[0065] 2. The acupuncture structure C / SiC-HfB 2 -TaB 2 The patch material is designed as a trapezoidal hexahedron matching the groove of the component, and the component body and the patch material are connected by screws to complete the physical connection.

[0066] 3. Use high-temperature adhesive to coat all connecting parts and surfaces. The adhesive contains Si, C, O, and B, which can meet the requirements of 1200°C.

[0067] 4. Install patch.

[0068] 5. Use the PIP process for online connection. The solution used is the SiBCN precursor solution. Repeat the PIP process 4 times to complete the reinforcement.

[0069] Acupuncture the present embodiment C / SiC-HfB 2 -TaB 2 The continuous carbon ...

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PUM

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Abstract

The invention relates to the technical field of ceramic composite materials, and provides a reinforcing method of a continuous carbon fiber toughened ceramic matrix composite material. The reinforcing method comprises the following steps: connecting the connecting parts of continuous carbon fiber toughened ceramic matrix composite material components by using a patch material to complete the reinforcing. According to the method, the patch with better ablation resistance is adopted to reinforce the component, the patch is ablated firstly in the test, and the component below is not ablated or is ablated slightly, so that the continuity of carbon fibers of the whole component is ensured, and the use performance of the whole component is effectively improved. Compared with patches made of the same material as the component, the patch used in the invention can adapt to a more stringent test environment; under the same test environment, the patch used in the invention is smaller in size and lighter in weight; and the applicable use environment range is wide.

Description

technical field [0001] The invention relates to the technical field of ceramic composite materials, in particular to a reinforcement method for continuous carbon fiber toughened ceramic matrix composite materials. Background technique [0002] Continuous carbon fiber toughened silicon carbide ceramic matrix composite is an ideal high-temperature structural material, which has a series of advantages such as high temperature resistance, low density, high strength, and thermal shock resistance. It has a wide range of applications and prospects in the aerospace field. When continuous carbon fiber toughened silicon carbide ceramic matrix composites are used in high-temperature air flow and particle erosion environments, the components will suffer from wear and oxidation damage, resulting in damage to the components and making them unable to continue to be used. During the service of composite components, usually only the parts with the most severe local service conditions (such a...

Claims

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Application Information

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IPC IPC(8): B28B11/08B28B11/02B28B11/22
CPCB28B11/08B28B11/22B28B11/02Y02T50/40
Inventor 金鑫霍鹏飞刘俊鹏左红军于艺杨良伟李晓东于新民杨冰洋
Owner AEROSPACE INST OF ADVANCED MATERIALS & PROCESSING TECH
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