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Polyether-ether-ketone and preparation method thereof

A technology of polyetheretherketone and fluoroketone, applied in the field of polyetheretherketone and its preparation

Active Publication Date: 2022-01-11
JILIN ZHONGYAN HIGH PERFORMANCE PLASTIC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, polyetheretherketone with a whiter color is needed in specific fields, so the current polyetheretherketone and its preparation method still need further improvement

Method used

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  • Polyether-ether-ketone and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0064] Add 300g of hydroquinone to a 500ml four-necked bottle, insert a stirring paddle into the middle port of the four-necked bottle, insert a tee pipe into one side port, connect the thermometer and argon gas inlet respectively to the three-way pipe, and insert a side port into The ventilation pipe is connected to the bottom of the four-necked bottle, and one side port is connected with a spherical condenser as an exhaust port. Put the four-necked bottle into the electric heating mantle, and pass high-purity argon gas into the four-necked bottle from the two inlet ports. The flow rate of argon gas is 50ml / min, and the purity of argon gas is ≥99.999%. Turn on the heating until the hydroquinone melts, adjust the argon gas flow to 200ml / min, start the stirring speed to 80rpm, maintain the temperature of the molten hydroquinone at 178°C, and continue the reaction for 1 hour. Put the four-neck bottle into a hot oil bath and cool to room temperature, turn off the argon to obtain ...

Embodiment 2

[0067]Add 300g of hydroquinone to a 500ml four-necked bottle, insert a stirring paddle into the middle port of the four-necked bottle, insert a tee pipe into one side port, connect the thermometer and argon gas inlet respectively to the three-way pipe, and insert a side port into The ventilation pipe is connected to the bottom of the four-necked bottle, and one side port is connected with a spherical condenser as an exhaust port. Put the four-necked bottle into the electric heating mantle, and pass high-purity argon gas into the four-necked bottle from the two inlet ports. The flow rate of argon gas is 50ml / min, and the purity of argon gas is ≥99.999%. Turn on the heating until the hydroquinone melts, adjust the argon gas flow rate to 200ml / min, start the stirring speed to 80rpm, maintain the temperature of the molten hydroquinone liquid at 188°C, and continue the reaction for 1 hour. Put the four-neck bottle into a hot oil bath to cool to room temperature, turn off the argon ...

Embodiment 3

[0070] Add 300g of hydroquinone to a 500ml four-necked bottle, insert a stirring paddle into the middle port of the four-necked bottle, insert a tee pipe into one side port, connect the thermometer and argon gas inlet respectively to the three-way pipe, and insert a side port into The ventilation pipe is connected to the bottom of the four-necked bottle, and one side port is connected with a spherical condenser as an exhaust port. Put the four-necked bottle into the electric heating mantle, and pass high-purity argon gas into the four-necked bottle from the two inlet ports. The flow rate of argon gas is 50ml / min, and the purity of argon gas is ≥99.999%. Turn on the heating until the hydroquinone melts, adjust the argon gas flow to 200ml / min, start the stirring speed to 80rpm, maintain the temperature of the molten hydroquinone at 198°C, and continue the reaction for 1 hour. Put the four-neck bottle into a hot oil bath to cool to room temperature, turn off the argon to obtain t...

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PUM

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Abstract

The invention provides polyether-ether-ketone and a preparation method thereof. The method comprises the following steps: introducing argon into a container containing the bisphenol compound to obtain a complex of the bisphenol compound; and mixing fluoroketone, alkali carbonate, the complex of the bisphenol compound and a solvent, and carrying out temperature programming treatment on the mixture to generate the polyether-ether-ketone. Therefore, before the polyether-ether-ketone is prepared, the bisphenol compound is protected by argon, so that the bisphenol compound cannot be oxidized into quinones when the bisphenol compound reacts with fluoroketone and alkali carbonate, and a whiter polyether-ether-ketone solid with a higher chromatic value L*can be obtained.

Description

technical field [0001] The invention relates to the field of polymer materials, in particular to polyether ether ketone and a preparation method thereof. Background technique [0002] Poly(aryl ether ketone) polymer is an aromatic linear polymer material. It is a new type of semi-crystalline aromatic thermoplastic engineering plastic successfully researched and developed in the late 1970s. It has high temperature resistance, chemical resistance, high Strength, high modulus, high fracture toughness and excellent dimensional stability, etc. A typical representative of poly(aryl ether ketone) polymers is polyetheretherketone, which has a glass transition temperature (Tg) of 143°C, a melting point of 334°C, and a maximum attainable crystallinity of 48%, generally 20%. ~30%. Its density in the amorphous state is 1.265g / cm 3 , the density at the maximum crystallinity is 1.32g / cm 3 . Its crystalline form makes it have outstanding heat resistance and mechanical properties. The ...

Claims

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Application Information

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IPC IPC(8): C08G8/02
CPCC08G8/02C08G65/4012C08G65/4093C08G65/46C08G2650/40
Inventor 谢怀杰平仕衡
Owner JILIN ZHONGYAN HIGH PERFORMANCE PLASTIC
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