Oil-displacing discharge aiding agent as well as preparation method and application thereof
A technology of drainage aid and oil displacement, which is applied in the preparation of ether, sulfonic acid, and sulfate, etc., and can solve the problems of limited and poor development effect.
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[0020] In a typical implementation of the present application, a method for preparing an oil displacement aid is provided, the preparation method comprising: step S1, mixing coniferyl alcohol, ethylene oxide and the first solvent under alkaline conditions Carry out ring-opening reaction, obtain ring-opening compound; Step S2, ring-opening compound, SO 3 and the second solvent for a sulfonation reaction to obtain a sulfonate compound; step S3, mixing the sulfonate compound and a surface active substance to obtain an oil displacement aid; wherein the surface active substance is a fluorocarbon surfactant and a carbonic acid The mixture of ammonium hydrogen, the ring-opening compound and the sulfonate compound have the following structural formulas respectively:
[0021]
[0022] m + is a monovalent cation.
[0023] The application utilizes coniferyl alcohol and ethylene oxide in alkaline conditions (M + For the ring-opening reaction from the cation in the alkaline condition...
Embodiment 1
[0039] Take 1g of coniferyl alcohol, 2g of ethylene oxide, and 0.1g of sodium hydroxide in a 25mL three-necked flask, and add 10mL of dioxane solvent, and carry out the ring-opening reaction at 80°C for 5h, and wait until the temperature of the system drops to At room temperature, add water and wash it for 3 times to obtain a product system comprising a ring-opening compound; mix the product system comprising a ring-opening compound with 0.5gSO 3 10mL of dioxane solvent was subjected to sulfonation reaction at room temperature for 6h, and then extracted to obtain sodium sulfonate compound; 0.1g of fluorocarbon surfactant was mixed with 2g of ammonium bicarbonate to obtain surface active substances, and then Take 0.3g sodium sulfonate compound and 0.2g surface active substance and mix uniformly to obtain oil displacement aid drainage agent 1.
Embodiment 2
[0041] Take 1g coniferyl alcohol, 1g ethylene oxide, 0.15g sodium hydroxide, and carry out the ring-opening reaction at 85°C for 4h, wait for the temperature of the system to drop to room temperature, add water and wash it three times to obtain The product system of compound; Obtain the product system that comprises ring-opening compound; The product system that comprises ring-opening compound and 1gSO 3 10mL of dioxane solvent was subjected to sulfonation reaction at room temperature for 4h, and then extracted to obtain sodium sulfonate compound; 0.1g of fluorocarbon surfactant was mixed with 2g of ammonium bicarbonate to obtain surface active substances, and then Take 0.3g sodium sulfonate compound and 0.2g surface active substance and mix uniformly to obtain oil displacement aid 2.
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