Long-acting easy-to-clean sunscreen cream and preparation method thereof
A sunscreen and easy-to-clean technology, applied in the direction of medical preparations containing active ingredients, skin care preparations, pharmaceutical formulas, etc., can solve the problems of short residence time, poor sun protection durability, easy to fall off, etc., to improve adhesion, The effect of prolonging the sun protection time
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Embodiment 1
[0032] A long-acting and easy-to-clean sunscreen, including the following components in mass percentages: titanium dioxide@formylated chondroitin sulfate / gelatin 15%, octocrylene 3%, ethylhexyl triazone 1%, butylmethoxy Dibenzoylmethane 3%, Sorbitan Sesquioleate 3%, Methyl Methacrylate Crosspolymer 0.5%, Bakelyl Alcohol 1.5%, Caprylic / Capric Triglyceride 1.5%, Panthenol 1.5 %, betaine 2.5%, sodium hyaluronate 6%, and the balance is water.
[0033] The preparation method of the titanium dioxide@formylated chondroitin sulfate / gelatin is as follows:
[0034] (A) placing titanium dioxide in a ball mill, and ball milling for 3 hours at a temperature of 100° C. and a rotational speed of the ball mill of 500 r / min to obtain pretreated titanium dioxide;
[0035] (B) In the dark, at 25°C, add 5.5wt% sodium periodate solution dropwise while stirring in 9wt% chondroitin sulfate solution, between the chondroitin sulfate solution and sodium periodate solution The volume ratio is 10:1. Af...
Embodiment 2
[0043] A long-acting and easy-to-clean sunscreen, comprising the following components in mass percentages: titanium dioxide@formylated chondroitin sulfate / gelatin 18%, phenylbenzimidazole sulfonic acid 0.6%, ethylhexyl salicylate 1 %, Bis-Ethylhexyloxyphenol Methoxyphenyl Triazine 1.9%, Polyhydroxystearic Acid 4%, Tapioca Starch 0.6%, Caprylic / Capric Triglyceride 2.5%, Squalane 4%, 1,2 - Hexylene glycol 1%, betaine 3.5%, sodium hyaluronate 2.5%, balance water.
[0044] The preparation method of the titanium dioxide@formylated chondroitin sulfate / gelatin is as follows:
[0045] (A) Titanium dioxide is placed in a ball mill, and ball milled for 2 hours at a temperature of 150° C. and a rotational speed of the ball mill of 400 r / min to obtain pretreated titanium dioxide;
[0046] (B) In the dark, at 30°C, add 4.5wt% sodium periodate solution dropwise while stirring in 11wt% chondroitin sulfate solution, between the chondroitin sulfate solution and sodium periodate solution The ...
Embodiment 3
[0054] A long-lasting and easy-to-clean sunscreen, including the following components in mass percentages: titanium dioxide@formylated chondroitin sulfate / gelatin 20%, cetearyl glucoside 5%, carbomer 0.8%, shark liver Alcohol 4%, Caprylic / Capric Triglyceride 2.6%, Squalane 3.4%, Panthenol 1.5%, Betaine 3.5%, balance water.
[0055] The preparation method of the titanium dioxide@formylated chondroitin sulfate / gelatin is as follows:
[0056] (A) Put titanium dioxide in a ball mill, and ball mill for 1 hour at a temperature of 200° C. and a rotation speed of the ball mill of 300 r / min to obtain pretreated titanium dioxide;
[0057] (B) In the dark, at 35°C, add 3.5wt% sodium periodate solution dropwise while stirring in 13wt% chondroitin sulfate solution, between the chondroitin sulfate solution and sodium periodate solution The volume ratio of the solution is 8:1. After the dropwise addition, continue to react at 35°C for 3.5 hours, add ethylene glycol to terminate the reaction...
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