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Binder-free preparation method for preparing composite carbon-based fertilizer by using biogas residues

A technology of compound carbon and biochar base fertilizer, applied in urea compound fertilizer, application, potash fertilizer and other directions, can solve the problems of non-binder biochar base fertilizer not easy to form, low utilization rate of chemical fertilizer, low hardness, etc. Sustained development, lower production cost, good compression effect

Pending Publication Date: 2021-08-20
SHANGHAI JIAO TONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] In order to overcome the deficiencies of the prior art, the object of the present invention is to provide a method for preparing composite carbon-based fertilizer particles from biogas residue without adding a binder. The defects of low-yield biochar-based fertilizers, which are not easy to form and have low hardness, solve the problem of low utilization rate of traditional chemical fertilizers

Method used

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  • Binder-free preparation method for preparing composite carbon-based fertilizer by using biogas residues
  • Binder-free preparation method for preparing composite carbon-based fertilizer by using biogas residues
  • Binder-free preparation method for preparing composite carbon-based fertilizer by using biogas residues

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preparation example Construction

[0044] Embodiment 1-5 adopts the preparation method as described below to prepare:

[0045] Pretreatment: Collect biogas residue after solid-liquid separation, air-dry and pulverize to obtain dry biogas residue powder;

[0046] High-temperature pyrolysis: transfer the dried biogas residue powder obtained from pretreatment into a muffle furnace, and perform pyrolysis for a period of time under the conditions of pyrolysis temperature to obtain biogas residue biochar materials;

[0047] Preparation of biogas residue carbon-based compound fertilizer: The biogas residue biochar material obtained by high-temperature pyrolysis is uniformly mixed with urea, diammonium hydrogen phosphate, potassium chloride and distilled water in a certain proportion to prepare a composite biogas residue biochar-based fertilizer.

[0048] Granulation preparation: the prepared composite biochar residue biochar-based fertilizer is placed in an extrusion granulator, and granulated under certain compressio...

Embodiment 1

[0062] Biogas residue carbon-based compound fertilizer: 35 parts of biogas residue biochar, 28 parts of urea, 20 parts of diammonium hydrogen phosphate, 20 parts of potassium chloride, 7.5 parts of distilled water, and uniformly mixed to prepare a composite biogas residue biochar-based fertilizer.

[0063] Granulation preparation: put the prepared biogas residue carbon-based compound fertilizer in an extrusion granulator with a sleeve diameter of 7mm, and granulate under the conditions of a compression speed of 50mm / min and a pressure of 7.5Mpa to obtain a granular form Composite biochar residue biochar fertilizer.

[0064] Granular drying: The prepared granular composite biochar-based fertilizer was dried at 25°C for 8 hours.

Embodiment 2

[0066] Biogas residue carbon-based compound fertilizer: 40 parts of biogas residue biochar, 30 parts of urea, 22 parts of diammonium hydrogen phosphate, 22 parts of potassium chloride, 5 parts of distilled water, and uniformly mixed to prepare a composite biogas residue biochar-based fertilizer.

[0067] Granulation preparation: put the prepared biogas residue carbon-based compound fertilizer in an extrusion granulator with a sleeve diameter of 7mm, and granulate under the conditions of a compression speed of 60mm / min and a pressure of 7.5Mpa to obtain a granule Composite biochar residue biochar fertilizer.

[0068] Granular drying: The prepared granular composite biochar-based fertilizer was dried at 65°C for 8 hours.

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Abstract

The invention discloses a binder-free preparation method for preparing a composite carbon-based fertilizer by using biogas residues, which comprises the steps of conducting pretreatment, specifically, collecting biogas residues after solid-liquid separation, air-drying and crushing to obtain dried biogas residue powder; performing high-temperature pyrolysis, specifically, transferring the pretreated dried biogas residue powder into a muffle furnace, and performing pyrolysis for a period of time under a pyrolysis temperature condition to obtain a biogas residue biochar material; preparing a biogas residue carbon-based compound fertilizer; and carrying out granulation preparation, specifically, placing the prepared composite biogas residue biochar base fertilizer in an extrusion die, and performing granulation under certain compression speed and pressure conditions to obtain the granular composite biogas residue biochar base fertilizer. The biogas residues are utilized for reproduction, and the environmental and economic burden is relieved; the process is simple, and the cost is low; a binder is not added, so that the method is environment-friendly; powder is granulated, so that the transportation and application difficulties are solved; and meanwhile, the granules are dried at high temperature after being formed, nutrients are tightly combined with charcoal functional groups, the nutrient release time is prolonged, and the fertilizer quality is improved.

Description

technical field [0001] The invention belongs to the technical field of agricultural fertilizers, and in particular relates to a binder-free biogas residue carbon-based fertilizer particle and a preparation method thereof. Background technique [0002] With the increase of the global population, a large amount of kitchen waste is produced, causing potential environmental and economic burdens. Anaerobic fermentation, as an environmentally friendly way to deal with food waste, is due to its use in renewable energy production and waste reuse. potential has received increasing attention. However, the treatment of food waste anaerobic fermentation residue biogas residues has always been a difficult problem to solve. Domestically, there have been patent applications for using biogas residues as raw materials to make fertilizers, such as: [0003] The publication number is CN101423425A, and the publication date is May 6, 2009. The Chinese patent document entitled "Comprehensive Ut...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C05G3/40C05G5/12
CPCC05G3/40C05G5/12C05B7/00C05C9/00C05D1/02C05D9/00
Inventor 沈国清余洲李晓颖陈钦程孙鹏王晨谭棋仁
Owner SHANGHAI JIAO TONG UNIV
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