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Liquid-metal thermal interface material with self-packaging function and preparation method thereof

A technology of thermal interface material and liquid metal, applied in the direction of heat exchange materials, chemical instruments and methods, etc., can solve the problems of high fluidity of liquid metal, short circuit, etc., achieve no fluidity, not easy to leak, and reduce contact heat The effect of resistance

Active Publication Date: 2021-06-18
GRIMAT ENG INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Patent CN103722804A proposes a multi-layer structure double-melting point liquid metal thermal interface material, and patent CN108329830A proposes a thermal interface material that combines liquid metal and silicone grease, both to solve the problem of high fluidity of liquid metal after melting, which is easy to cause circuit short circuit And other issues

Method used

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Examples

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preparation example Construction

[0023] The preparation method of the liquid metal thermal interface material with self-encapsulation function of the present invention comprises the following process steps:

[0024] (1) Pretreatment of raw materials: Ultrasonic cleaning of high melting point liquid metal powder, low melting point liquid metal powder, and high thermal conductivity filler in ethanol for 20-40 minutes, then ultrasonic cleaning in deionized water for 20-40 minutes, and then filtering and drying , weighed according to the required ratio;

[0025] (2) Place the prepared mixed powder in an ultrasonic oscillator, add deionized water at a volume ratio of 1:1, and ultrasonically vibrate for 30 to 60 minutes to make high melting point liquid metal powder, low melting point liquid metal powder, and high thermal conductivity filler particles Mix well, then filter and dry;

[0026] (3) Place the obtained mixed powder in a hot pressing mold at a mold temperature of 50-120° C., and press the powder into a s...

Embodiment 1

[0029] The liquid metal thermal interface material with self-encapsulation function in this embodiment 1 includes the following components in volume percentage: 70 vol% of the liquid metal part; 30 vol% of the high thermal conductivity filler part. The liquid metal part is a mixture of two liquid metals with different melting points. The high melting point liquid metal adopts 86Sn-9Zn-5Bi, the low melting point liquid metal adopts 49Bi-21In-18Pb-12Sn, and the volume ratio of high melting point liquid metal and low melting point liquid metal is 1:1. The high thermal conductivity filler selected is nano-diamond with a particle size of 100-300nm.

[0030] The preparation method of the liquid metal thermal interface material with self-encapsulation function includes the following process steps:

[0031] (1) Pre-treatment of raw materials: Ultrasonic cleaning of high melting point liquid metal 86Sn-9Zn-5Bi, low melting point liquid metal 49Bi-21In-18Pb-12Sn, and nano-diamond in et...

Embodiment 2

[0037] In Example 2, the liquid metal thermal interface material with self-encapsulation function contains the following components in volume percentage: 94 vol% of the liquid metal part; 6 vol% of the high thermal conductivity filler part. The liquid metal part is a mixture of two liquid metals with different melting points. The high melting point liquid metal adopts 91Sn-9Zn, the low melting point liquid metal adopts 27Sn-44.9In-28.1Bi, and the volume ratio of high melting point liquid metal and low melting point liquid metal is 1:1. The selected high thermal conductivity filler is carbon nanotube with a particle size of 100-200nm.

[0038] The preparation method of the liquid metal thermal interface material with self-encapsulation function includes the following process steps:

[0039] (1) Pretreatment of the raw materials used: Ultrasonic cleaning of high melting point liquid metal 91Sn-9Zn, low melting point liquid metal 27Sn-44.9In-28.1Bi, and carbon nanotubes in ethan...

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Abstract

The invention relates to a liquid-metal thermal interface material with a self-packaging function and a preparation method thereof, and belongs to the technical field of thermal interface materials. In the thermal interface material, liquid metal accounts for 70 vol%-99 vol%; and high thermal conductivity filler accounts for 1 vol%-30 vol%. The liquid metal is formed by mixing two or more kinds of liquid metal with different melting points. The preparation method comprises the following steps that raw materials are cleaned, mixed, and then put into an ultrasonic processor, deionized water is added, ultrasonic treatment is carried out, and then filtering and drying are carried out; and then, the mixture is subjected to hot-pressing into a sheet shape, and finish rolling is carried out to obtain the sheet-shaped thermal interface material. According to the liquid-metal thermal interface material, at a use temperature, the high-melting-point part is in a solid state, the low-melting-point part is in a liquid state, the solid-phase part limits flowing of the liquid phase, the self-packaging effect is achieved, and the liquid-metal thermal interface material has a state of softening paraffin and has high flexibility and no fluidity. In addition, the liquid-metal thermal interface material has a high thermal conductivity (greater than 60 W / mK) and good processability. 60 W / mK) and good processability.

Description

technical field [0001] The invention belongs to the technical field of thermal interface materials, and in particular relates to a liquid metal thermal interface material with self-encapsulation function and a preparation method thereof. Background technique [0002] With the development of information electronics technology, electronic devices are showing a trend of miniaturization, thinning, and high integration, and their power density and calorific value are also continuously increasing, which puts forward higher requirements for thermal management materials and technologies. The problem of heat dissipation has become a bottleneck problem in the development of microelectronics technology, and the contact thermal resistance between components in electronic devices is an obstacle that restricts the rapid transfer of heat outward. An effective way of interfacial contact thermal resistance. [0003] At present, the common thermal interface material in the market is thermal ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C30/00C09K5/06C22C12/00C22C28/00C22C1/04
CPCC22C30/00C22C12/00C22C28/00C09K5/06C22C1/04C22C1/0483
Inventor 郭宏谢忠南张习敏
Owner GRIMAT ENG INST CO LTD
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