Liquid-metal thermal interface material with self-packaging function and preparation method thereof
A technology of thermal interface material and liquid metal, applied in the direction of heat exchange materials, chemical instruments and methods, etc., can solve the problems of high fluidity of liquid metal, short circuit, etc., achieve no fluidity, not easy to leak, and reduce contact heat The effect of resistance
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[0023] The preparation method of the liquid metal thermal interface material with self-encapsulation function of the present invention comprises the following process steps:
[0024] (1) Pretreatment of raw materials: Ultrasonic cleaning of high melting point liquid metal powder, low melting point liquid metal powder, and high thermal conductivity filler in ethanol for 20-40 minutes, then ultrasonic cleaning in deionized water for 20-40 minutes, and then filtering and drying , weighed according to the required ratio;
[0025] (2) Place the prepared mixed powder in an ultrasonic oscillator, add deionized water at a volume ratio of 1:1, and ultrasonically vibrate for 30 to 60 minutes to make high melting point liquid metal powder, low melting point liquid metal powder, and high thermal conductivity filler particles Mix well, then filter and dry;
[0026] (3) Place the obtained mixed powder in a hot pressing mold at a mold temperature of 50-120° C., and press the powder into a s...
Embodiment 1
[0029] The liquid metal thermal interface material with self-encapsulation function in this embodiment 1 includes the following components in volume percentage: 70 vol% of the liquid metal part; 30 vol% of the high thermal conductivity filler part. The liquid metal part is a mixture of two liquid metals with different melting points. The high melting point liquid metal adopts 86Sn-9Zn-5Bi, the low melting point liquid metal adopts 49Bi-21In-18Pb-12Sn, and the volume ratio of high melting point liquid metal and low melting point liquid metal is 1:1. The high thermal conductivity filler selected is nano-diamond with a particle size of 100-300nm.
[0030] The preparation method of the liquid metal thermal interface material with self-encapsulation function includes the following process steps:
[0031] (1) Pre-treatment of raw materials: Ultrasonic cleaning of high melting point liquid metal 86Sn-9Zn-5Bi, low melting point liquid metal 49Bi-21In-18Pb-12Sn, and nano-diamond in et...
Embodiment 2
[0037] In Example 2, the liquid metal thermal interface material with self-encapsulation function contains the following components in volume percentage: 94 vol% of the liquid metal part; 6 vol% of the high thermal conductivity filler part. The liquid metal part is a mixture of two liquid metals with different melting points. The high melting point liquid metal adopts 91Sn-9Zn, the low melting point liquid metal adopts 27Sn-44.9In-28.1Bi, and the volume ratio of high melting point liquid metal and low melting point liquid metal is 1:1. The selected high thermal conductivity filler is carbon nanotube with a particle size of 100-200nm.
[0038] The preparation method of the liquid metal thermal interface material with self-encapsulation function includes the following process steps:
[0039] (1) Pretreatment of the raw materials used: Ultrasonic cleaning of high melting point liquid metal 91Sn-9Zn, low melting point liquid metal 27Sn-44.9In-28.1Bi, and carbon nanotubes in ethan...
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