Anti-dazzle self-repairing mobile phone screen protection film
A mobile phone screen, self-healing technology, applied in the field of mobile phone screen protective film, can solve the problems affecting the overall appearance, tarnish, and brittleness of mobile phones, achieve effective disulfide bond transfer ability, promote aromatic disulfide bond exchange, enhance The effect of mechanical robustness
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Embodiment 1
[0029] A preparation method of an anti-glare self-repairing mobile phone screen protective film, comprising the steps of:
[0030] (1) Heat 70 parts of dehydrated polytetramethylene ether glycol to 70°C to make it into a molten state, and mix it with 9 parts of 2,2-bis(hydroxymethyl)propionic acid under vacuum at 40°C, Stirring time 30min, after the mixing is completed, add 22 parts of isophorone diisocyanate to the mixture and continue to stir for 1.5h under nitrogen protection, add 3 parts of methyl ethyl ketone and 2 parts of dibutyltin dilaurate after the stirring is finished, and Heat the mixture to 50°C and gradually add 8 parts of aromatic disulfide to the mixed solution and stir for 1 hour. After the reaction is completed and cooled to room temperature, add dimethylformamide dropwise and continue stirring for 2 hours. Put it in a vinyl mold, put it in a vacuum oven at 80°C for 24 hours under normal pressure to remove dimethylformamide, and finally dry it under vacuum a...
Embodiment 2
[0037] A preparation method of an anti-glare self-repairing mobile phone screen protective film, comprising the steps of:
[0038] (1) Heat 60 parts of dehydrated polytetramethylene ether glycol to 70°C to make it into a molten state and mix it with 8 parts of 2,2-bis(hydroxymethyl)propionic acid at 40°C under vacuum condition to mix evenly, Stirring time 30min, after the mixing is completed, add 20 parts of isophorone diisocyanate to the mixture and continue to stir for 1.5h under the protection of nitrogen, add 2 parts of butanone and 4 parts of dibutyltin dilaurate after the stirring is finished, and Heat the mixture to 50°C and gradually add 9 parts of aromatic disulfide to the mixed solution and stir for 1 hour. After the reaction is completed and cooled to room temperature, add dimethylformamide dropwise and continue stirring for 2 hours. Put it in a vinyl mold, put it in a vacuum oven at 80°C for 24 hours under normal pressure to remove dimethylformamide, and finally dr...
Embodiment 3
[0045]A preparation method of an anti-glare self-repairing mobile phone screen protective film, comprising the steps of:
[0046] (1) Heat 80 parts of dehydrated polytetramethylene ether glycol to 70°C to make it into a molten state and mix it with 12 parts of 2,2-bis(hydroxymethyl)propionic acid at 40°C under vacuum condition to mix evenly, Stirring time 30min, after the mixing is completed, add 25 parts of isophorone diisocyanate to the mixture and continue to stir for 1.5h under the protection of nitrogen, add 4 parts of butanone and 5 parts of dibutyltin dilaurate after stirring, and Heat the mixture to 50°C and gradually add 10 parts of aromatic disulfide to the mixed solution and stir for 1 hour. After the reaction is completed and cooled to room temperature, add dimethylformamide dropwise and continue stirring for 2 hours. Put it into a vinyl mold, put it in a vacuum oven at 80°C for 24 hours under normal pressure to remove dimethylformamide, and finally dry it under va...
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