Mild discharge preparation method and device of fluorinated graphene
A technology of fluorinated graphene and preparation device, applied in chemical instruments and methods, graphene, inorganic chemistry, etc., can solve problems such as complicated preparation operations, and achieve the effects of wide source of raw materials, low energy consumption, and reduced preparation costs
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[0029] Embodiments of the present invention are described in detail below, examples of which are shown in the drawings, wherein the same or similar reference numerals designate the same or similar elements or elements having the same or similar functions throughout. The embodiments described below by referring to the figures are exemplary only for explaining the present invention and should not be construed as limiting the present invention.
[0030] refer to figure 1 Shown, the present invention discloses a kind of gentle discharge preparation method of fluorinated graphene, comprises the following steps:
[0031] S1: Mix the carbon source, polytetrafluoroethylene powder and active metal with a melting point higher than 450° C. and place them in the reaction tube 102 .
[0032] S2: Passing an inert gas into the reaction tube 102 . Specifically, an inert gas such as any of argon or nitrogen.
[0033] S3: Preheat the mixture according to the set voltage value and capacitance...
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