Ferrite-coated FeSiAl metal magnetic powder core and preparation method thereof
A technology of ferrite and magnetic powder cores, applied in the field of ferrite-coated FeSiAl metal magnetic powder cores and its preparation, can solve the problems of easy cracking of the Mn-Zn ferrite insulating layer, increased eddy current loss, and reduced energy consumption , to achieve the effect of reducing magnetic dilution, reducing magnetic dilution, and solving the effect of large eddy current loss
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Embodiment 1
[0039] (1) Mix FeSiAl metal soft magnetic powder with FeCl 2 mixed with the aqueous solution of FeSiAl, heated to 80 °C, heated and stirred for 20 min, so that a layer of soluble FeCl was formed on the surface of FeSiAl metal soft magnetic powder. 2 , and dried at 90℃ for 20min to obtain FeSiAl metal soft magnetic powder@FeCl 2 ;Based on the total mass of FeSiAl metal soft magnetic powder, FeCl 2 The addition amount is 1wt%;
[0040] (2) The FeSiAl metal soft magnetic powder obtained in step (1) @FeCl 2 Mix with NaOH solution, stir evenly at room temperature (20°C), and dry at 90°C for 20 minutes to obtain insulating metal soft magnetic powder; based on the total mass of FeSiAl metal soft magnetic powder, the amount of NaOH added is 2wt%;
[0041] (3) Mix the insulating metal soft magnetic powder obtained in step (2) with epoxy resin and zinc stearate uniformly, press and form under 1500MPa pressure to obtain a blank with an outer diameter of 33.00mm, an inner diameter of 1...
Embodiment 2
[0045] (1) Mix FeSiAl metal soft magnetic powder with FeCl 2 mixed with the aqueous solution of FeSiAl metal powder, heated to 100 °C, heated and stirred for 40 min, so that a layer of soluble FeCl was formed on the surface of FeSiAl metal soft magnetic powder. 2 , and dried at 120 °C for 40 min to obtain FeSiAl metal soft magnetic powder@FeCl 2 ;Based on the total mass of FeSiAl metal soft magnetic powder, FeCl 2 The addition amount is 3wt%;
[0046] (2) The FeSiAl metal soft magnetic powder obtained in step (1) @FeCl 2 Mix with NaOH solution, stir evenly at room temperature (40°C), and dry at 120°C for 40 minutes to obtain insulating metal soft magnetic powder; based on the total mass of FeSiAl metal soft magnetic powder, the amount of NaOH added is 3wt%;
[0047] (3) Mixing the insulating metal soft magnetic powder obtained in step (2) with epoxy resin and zinc stearate uniformly, press molding under 2000MPa pressure to obtain a blank with an outer diameter of 33.00mm, a...
Embodiment 3
[0051] (1) The FeSiAl metal soft magnetic powder and FeSO 4 mixed with the aqueous solution of FeSiAl, heated to 80 °C, heated and stirred for 20 min to form a layer of soluble FeSO on the surface of FeSiAl metal soft magnetic powder 4 , and dried at 90℃ for 20min to obtain FeSiAl metal soft magnetic powder@FeSO 4 ;Based on the total mass of FeSiAl metal soft magnetic powder, FeSO 4 The addition amount is 1wt%;
[0052] (2) The FeSiAl metal soft magnetic powder obtained in step (1) @FeCl 2 Mix with KOH solution, stir evenly at room temperature, and dry at 90°C for 20 minutes to obtain insulating metal soft magnetic powder; based on the total mass of FeSiAl metal soft magnetic powder, the amount of KOH added is 2wt%;
[0053] (3) Mixing the insulating metal soft magnetic powder obtained in step (2) with water glass, barium stearate and zinc stearate uniformly, and pressing under pressure of 1500~2000MPa to obtain an outer diameter of 33.00mm and an inner diameter of 19.90mm ...
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