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Preparation method for antibacterial melt-blown non-woven fabric

A technology of melt-blown non-woven fabrics and polypropylene non-woven fabrics, which is applied in the processing of textile materials, textiles and papermaking, liquid/gas/steam textile material processing, etc. It can solve the problems of non-antibacterial properties and achieve a fluffy structure , many gaps, the effect of improving efficiency

Active Publication Date: 2020-07-17
FUJIAN HENGAN HLDG CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Therefore, in view of the above content, the present invention provides a preparation method of antibacterial melt-blown non-woven fabric, which solves the problem that the prior art melt-blown non-woven fabric only has a high-efficiency filtering effect and does not have antibacterial properties.

Method used

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  • Preparation method for antibacterial melt-blown non-woven fabric
  • Preparation method for antibacterial melt-blown non-woven fabric

Examples

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Effect test

Embodiment 1

[0026] A preparation method for an antibacterial melt-blown nonwoven fabric, comprising the following steps:

[0027] (1) Preparation of modified polypropylene nonwoven fabric:

[0028]First, the polypropylene non-woven fabric is subjected to oxygen plasma treatment, the plasma power is 150W, and the treatment time is 400s. After the treatment, it is taken out, and then the methanol solution of 4-vinylbenzyl glycidyl ether with a mass fraction of 5% is sprayed on the polypropylene. The surface of the propylene non-woven fabric is grafted and modified by irradiating the polypropylene non-woven fabric with ultraviolet light using ultraviolet radiation technology. After 10 minutes of ultraviolet light irradiation, it is cleaned with ethanol ultrasonically, and then the polypropylene non-woven fabric is put into polyhexamethylene In the aqueous solution of guanidine phosphate, the molar ratio of 4-vinylbenzyl glycidyl ether to polyhexamethylene guanidine phosphate is 1:1.2, reflux...

Embodiment 2

[0034] A preparation method for an antibacterial melt-blown nonwoven fabric, comprising the following steps:

[0035] (1) Preparation of modified polypropylene nonwoven fabric:

[0036] First, the polypropylene non-woven fabric is subjected to oxygen plasma treatment, the plasma power is 200W, and the treatment time is 300s. After the treatment, it is taken out, and then the methanol solution of 4-vinylbenzyl glycidyl ether with a mass fraction of 5% is sprayed on the polypropylene. The surface of the propylene non-woven fabric is grafted and modified by irradiating the polypropylene non-woven fabric with ultraviolet light using ultraviolet radiation technology. After 15 minutes of ultraviolet light irradiation, it is cleaned with ethanol ultrasonically, and then the polypropylene non-woven fabric is put into polyhexamethylene In the aqueous solution of guanidine phosphate, the molar ratio of 4-vinylbenzyl glycidyl ether to polyhexamethylene guanidine phosphate is 1:1.3, reflu...

Embodiment 3

[0042] A preparation method for an antibacterial melt-blown nonwoven fabric, comprising the following steps:

[0043] (1) Preparation of modified polypropylene nonwoven fabric:

[0044] First, the polypropylene non-woven fabric is subjected to oxygen plasma treatment, the plasma power is 250W, and the treatment time is 200s. After the treatment, it is taken out, and then the methanol solution of 4-vinylbenzyl glycidyl ether with a mass fraction of 5% is sprayed on the polypropylene. The surface of the propylene non-woven fabric is grafted and modified by irradiating the polypropylene non-woven fabric with ultraviolet light by using ultraviolet radiation technology. In the aqueous solution of phosphate, the molar ratio of 4-vinylbenzyl glycidyl ether to polyhexamethyleneguanidine phosphate is 1:1.5, reflux reaction at 50°C for 12h, and ultrasonic cleaning with ethanol after the reaction. Obtain modified polypropylene non-woven fabric after vacuum drying;

[0045] (2) Preparat...

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Abstract

The invention relates to the technical field of non-woven fabrics, and provides a preparation method for an antibacterial melt-blown non-woven fabric. The preparation method comprises the following steps of (1) carrying out oxygen plasma treatment on a polypropylene non-woven fabric, and carrying out graft modification on the polypropylene non-woven fabric to prepare a modified polypropylene non-woven fabric; (2) polymerizing an amino-terminated hyperbranched polymer with propylene diamine and methyl methacrylate as raw materials, and preparing a modified hyperbranched polymer through polycondensation of carboxymethyl chitosan and the amino-terminated hyperbranched polymer; and (3) adding a copper chloride solution into a modified hyperbranched polymer aqueous solution, dropwise adding a sodium borohydride solution under nitrogen protection and ice bath conditions, carrying out impregnation treatment on the modified polypropylene non-woven fabric in the modified hyperbranched polymer aqueous solution after the reaction is finished, and drying to obtain the antibacterial melt-blown non-woven fabric. The preparation method solves a problem that the melt-blown non-woven fabric in theprior art only has an efficient filtering effect and does not have antibacterial property.

Description

technical field [0001] The invention relates to the technical field of non-woven fabrics, in particular to a method for preparing antibacterial melt-blown non-woven fabrics. Background technique [0002] The mask generally adopts SMS composite multi-layer structure, that is, the inner and outer layers are single-layer spunbond non-woven fabric, the middle layer is single-layer melt-blown non-woven fabric, or the middle layer is SMMS, which is multi-layer melt-blown non-woven fabric. SMMMS composite multilayer structure. The key to the filtering effect of the mask lies in the melt-blown non-woven fabric in the middle layer, which can filter micron-sized particles such as dust, microorganisms, and smog, and prevent the spread of germs. [0003] Melt-blown non-woven fabrics are made of polypropylene with high melt index as the main raw material, melted by high-pressure hot air flow, and then use high-speed hot air to draw the polymer melt stream extruded from the spinneret hol...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/37D06M11/83D06M10/00D06M14/28C08G81/00C08G83/00D06B3/10D06M101/20
CPCD06M15/37D06M11/83D06M16/00D06M10/00D06M14/28C08G81/00C08G83/006D06B3/10D06M2101/20
Inventor 汤国开姜慧勇黄阿玲
Owner FUJIAN HENGAN HLDG CO LTD
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