A kind of graphite negative electrode material, lithium ion battery and its preparation method and application
A graphite anode and raw material technology, applied in battery electrodes, secondary batteries, circuits, etc., can solve the problems of low charging capacity and poor low-temperature performance, and achieve the effects of high battery capacity, improved low-temperature electrical performance, and simple process
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Embodiment 1
[0056] In the crushing equipment, the calcined needle coke is crushed to obtain powder, the median particle size of the powder is controlled at 8-8.5 μm, the crushed material is shaped, and the shaped powder is mixed evenly . Under the protection of chlorine gas, the mixed powder was subjected to graphitization treatment. The graphitization temperature is 2900°C, and the graphitization time is 90h. The material after graphitization treatment is screened, and the mesh number of the screen is 250 mesh, to remove the lumps that coke quickly at high temperature during the graphitization process. Fully mix the sieved material with the binder asphalt according to the ratio of 100:3, and mix for 45 minutes, so that the asphalt is evenly distributed in the sieved material to prepare a mixture. The mixture was subjected to surface coating modification treatment, including two stages. The temperature of the first stage was 350°C and the time was 3h; the temperature of the second stage...
Embodiment 2
[0058] In the crushing equipment, the calcined needle coke is crushed to obtain powder, the median particle size of the powder is controlled at 8-8.5 μm, the crushed material is shaped, and the shaped powder is mixed evenly . Under the protection of chlorine gas, the mixed powder was subjected to graphitization treatment. The graphitization temperature is 2900°C, and the graphitization time is 90h. The material after graphitization treatment is screened, and the mesh number of the screen is 250 mesh, to remove the lumps that coke quickly at high temperature during the graphitization process. Fully mix the sieved material with the binder asphalt according to the ratio of 100:4, and mix for 45 minutes, so that the asphalt is evenly distributed in the sieved material to prepare a mixture. The mixture was subjected to surface coating modification treatment, including two stages. The temperature of the first stage was 350°C and the time was 3h; the temperature of the second stage...
Embodiment 3
[0061] In the crushing equipment, the calcined needle coke is crushed to obtain powder, the median particle size of the powder is controlled at 8-8.5 μm, the crushed material is shaped, and the shaped powder is mixed evenly . Under the protection of chlorine gas, the mixed powder was subjected to graphitization treatment. The graphitization temperature is 2900°C, and the graphitization time is 90h. The material after graphitization treatment is screened, and the mesh number of the screen is 250 mesh, to remove the lumps that coke quickly at high temperature during the graphitization process. Fully mix the sieved material with the binder asphalt according to the ratio of 100:5, and mix for 45 minutes, so that the asphalt is evenly distributed in the sieved material to prepare a mixture. The mixture was subjected to surface coating modification treatment, including two stages. The temperature of the first stage was 350°C and the time was 3h; the temperature of the second stage...
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