Magnetostrictive material and preparation method thereof
A technology of magnetostrictive materials and raw materials, which is applied in the direction of material selection and device material selection for magnetostrictive devices, and achieves the effects of easy process control, good magnetostrictive performance and comprehensive usability, and simple operation.
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Embodiment 1
[0032] A preparation method of the above-mentioned magnetostrictive material, comprising the following steps:
[0033] a. Weigh the raw materials according to the stoichiometric ratio Mn:Ni:Co:Si:Y:Eu=0.9:0.1:1:1:1:0.35, mix evenly, pour the prepared raw materials into a beaker, add distilled water to wash the raw materials, Pour off the distilled water;
[0034] b. Pour the raw materials into the copper crucible of the arc melting furnace. Put the elemental Zr into the copper crucible, number them sequentially, and close the furnace chamber. The electric arc furnace is cooled by a circulating water cooling system. Before smelting, use a mechanical pump to evacuate to below 9Pa, and then use a molecular pump to continue evacuating to 5×10 -5 Pa, turn off the molecular pump, fill with argon to 0.6 atmosphere. Start the vacuum arc melting furnace, first align the tungsten electrode with Zr, press the start button to start the arc, and then increase the current to 250A, and sta...
Embodiment 2
[0039] A preparation method of the above-mentioned magnetostrictive material, comprising the following steps:
[0040] a. Weigh the raw materials according to the stoichiometric ratio Mn:Ni:Co:Si:Y:Tm=0.92:0.08:1:1:1:0.22, mix evenly, pour the prepared raw materials into a beaker, add distilled water to wash the raw materials, Pour off the distilled water;
[0041] b. Pour the raw materials into the copper crucible of the arc melting furnace. Put the elemental Zr into the copper crucible, number them sequentially, and close the furnace chamber. The electric arc furnace is cooled by a circulating water cooling system. Before smelting, use a mechanical pump to evacuate to below 9Pa, and then use a molecular pump to continue evacuating to 5×10 -5 Pa, turn off the molecular pump, fill with argon to 0.6 atmosphere. Start the vacuum arc melting furnace, first align the tungsten electrode with Zr, press the start button to start the arc, and then increase the current to 250A, and...
Embodiment 3
[0046] A preparation method of the above-mentioned magnetostrictive material, comprising the following steps:
[0047] a. Weigh the raw materials according to the stoichiometric ratio Mn:Ni:Co:Si:Y:Ho=0.95:0.05:1:1:1:0.55, mix evenly, pour the prepared raw materials into a beaker, add distilled water to wash the raw materials, Pour off the distilled water;
[0048] b. Pour the raw materials into the copper crucible of the arc melting furnace. Put the elemental Zr into the copper crucible, number them sequentially, and close the furnace chamber. The electric arc furnace is cooled by a circulating water cooling system. Before smelting, use a mechanical pump to evacuate to below 9Pa, and then use a molecular pump to continue evacuating to 5×10 -5 Pa, turn off the molecular pump, fill with argon to 0.6 atmosphere. Start the vacuum arc melting furnace, first align the tungsten electrode with Zr, press the start button to start the arc, and then increase the current to 250A, and...
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