A kind of thermal interface composite material and its preparation method and application
A composite material and thermal interface technology, which is applied in the field of thermal interface composite materials and its preparation, can solve problems such as difficult processing, poor toughness, and reduced mechanical properties, and achieve excellent thermal conductivity and mechanical properties, high glass transition temperature, and improved surface area. The effect of external thermal conductivity
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Embodiment 1
[0067] This embodiment provides a thermal interface composite material, and the specific preparation method includes the following steps:
[0068](1) Preparation of carbon fiber skeleton: Mix 0.8 g of carbon fiber powder after surface hydrophilic treatment with an aqueous solution of binder, add appropriate amount of water to make a 3 mL suspension, first stir with a magnet, and then vacuum mix at a speed of 2000 rpm. Feed for 20 minutes to obtain a carbon fiber suspension with a volume percentage of carbon fibers of 12%; then freeze the carbon fiber suspension with liquid nitrogen and dry it in vacuum for 24 hours to obtain the carbon fiber skeleton in which the carbon fibers are arranged in a single orientation;
[0069] (2) Preparation of thermal interface composite material: The carbon fiber skeleton obtained in step (1) is completely immersed in epoxy resin, then placed in a vacuum drying oven, and vacuum filtered at 40°C for 3 hours; then gradient temperature rises and so...
Embodiment 2
[0073] This embodiment provides a thermal interface composite material, and the specific preparation method includes the following steps:
[0074] (1) Preparation of carbon fiber skeleton: Mix 0.8 g of carbon fiber powder after surface hydrophilic treatment with an aqueous solution of binder, add appropriate amount of water to make a 3 mL suspension, first stir with a magnet, and then vacuum mix at a speed of 1500 rpm. 10 min, the volume percentage of carbon fiber obtained was 12% of the carbon fiber suspension; then the carbon fiber suspension was frozen with liquid nitrogen and vacuum-dried for 12 hours to obtain the carbon fiber skeleton in which the carbon fibers were arranged in a single orientation;
[0075] (2) Preparation of thermal interface composite material: The carbon fiber skeleton obtained in step (1) is completely immersed in epoxy resin, then placed in a vacuum drying oven, and vacuum filtered at 30°C for 2 hours; then gradient temperature rises and solidifies ...
Embodiment 3
[0077] This embodiment provides a thermal interface composite material, and the specific preparation method includes the following steps:
[0078] (1) Preparation of carbon fiber skeleton: Mix 0.8 g of carbon fiber powder after surface hydrophilic treatment with an aqueous solution of binder, add appropriate amount of water to make a 3 mL suspension, first stir with a magnet, and then vacuum mix at a speed of 1800 rpm. 15min, the volume percentage of carbon fiber obtained was 12% of the carbon fiber suspension; then the carbon fiber suspension was frozen with liquid nitrogen and vacuum-dried for 20h to obtain the carbon fiber skeleton in which the carbon fibers were arranged in a single orientation;
[0079] (2) Preparation of thermal interface composite material: The carbon fiber skeleton obtained in step (1) is completely immersed in epoxy resin, then placed in a vacuum drying oven, and vacuum filtered at 35°C for 2.5h; then the temperature is gradually increased After curin...
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