Metal-carbon composite negative electrode material as well as preparation method and application thereof
A negative electrode material and metal technology, applied in the field of high-capacity lithium-ion battery negative electrode material and its preparation, can solve the problems of expensive raw materials, unsuitable production and application, complicated preparation process, etc.
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Embodiment 1
[0076] (1) Select coking coal with ash-free base volatile content of 15%, cohesive index of 52%, maximum thickness of colloidal layer of 25%, contained heteroatoms N, S, P and heteroatom content of 4% as raw material 100g of coking coal raw material dried at 120°C for 10h was put into a vibratory pulverizer for crushing for 1min, then ball milled for 6 hours in a planetary ball mill, sieved with a 500-mesh sieve, and the undersize was taken.
[0077] (2) Add 50 g of dried, crushed and sieved coking coal into a mixed acid solution with a mass ratio of hydrofluoric acid and sulfuric acid of 10:1, the liquid-solid ratio is 4, and the total acid concentration is adjusted to a pH value of 3 at room temperature. The mixture was stirred and reacted for 2 hours, filtered and washed until neutral to obtain acid-purified coke, and the ash content of the purified coke was 0.37%.
[0078] (3) Dissolve 10g of manganese acetate in 100ml of aqueous solution, add 20g of purified coke for ultr...
Embodiment 2
[0081] (1) Select coking coal with ash-free base volatile content of 25%, cohesive index of 62%, maximum thickness of colloidal layer of 25%, contained heteroatoms N, S, P and heteroatom content of 10% as raw material 100g of coking coal raw material dried at 120°C for 12h was put into a vibrating pulverizer for 10min, and then ball milled for 10 hours in a planetary ball mill, sieved with a 500-mesh sieve, and the undersize was taken.
[0082] (2) Add 50 g of dried, crushed and sieved coking coal into a mixed acid solution with a mass ratio of hydrofluoric acid and sulfuric acid of 2:1, the liquid-solid ratio is 6, and the total acid concentration is adjusted to a pH value of 4. The mixture was stirred and reacted for 5 hours, filtered and washed until neutral to obtain coke purified by acid method, and the ash content of the purified coke was 0.42%.
[0083] (3) Dissolve 20g of manganese acetate in 100ml of aqueous solution, add 1g of purified coke for ultrasonic dispersion ...
Embodiment 3
[0086] (1) Select coking coal with ash-free base volatile content of 20%, cohesive index of 58%, colloidal layer maximum thickness of 18%, contained heteroatoms N, S, P and heteroatom content of 8% as raw material 100g of bituminous coal raw material dried at 105°C for 10h was put into a vibratory pulverizer for crushing for 5min, then ball milled for 8 hours in a planetary ball mill, sieved with a 500-mesh sieve, and the undersize was taken.
[0087] (2) Add 50 g of dried, crushed and sieved coking coal into a mixed acid solution with a mass ratio of hydrofluoric acid and sulfuric acid of 10:1, the liquid-solid ratio is 5, and the total acid concentration is adjusted to a pH value of 3 at room temperature. The mixture was stirred and reacted for 5 hours, filtered and washed until neutral to obtain coke purified by acid method, and the ash content of the purified coke was 0.23%.
[0088] (3) Dissolve 10g of manganese acetate in 100ml of aqueous solution, add 50g of purified co...
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