A pretreatment solution and formation process for improving the capacity of medium and high voltage formation foils for aluminum electrolytic capacitors
A technology for aluminum electrolytic capacitors and pretreatment liquids, applied in electrolytic coatings, surface reaction electrolytic coatings, anodic oxidation, etc., can solve the problems of limited capacity of aluminum electrolytic capacitors and insufficient capacity of formed foils for aluminum electrolytic capacitors, and achieve stability The effects of high performance and competitiveness, weak electron mobility, and low leakage current
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Embodiment 1
[0035] Step 1: Take the 99.99% aluminum foil after electrolytic corrosion treatment and immerse it in pure water at 97°C for 20 minutes;
[0036] The second step: the pretreatment phosphoric acid concentration is 2ml / L, the sodium phytate concentration is 0.25g / L, the glucose concentration is 0.25g / L, the sodium bicarbonate concentration is 3.2g / L, the pH is 5.8, and the bath temperature is 70 ℃, treatment time 2 minutes;
[0037] The third step: in the first stage, the concentration of boric acid is 100g / L, the concentration of ammonium pentaborate is 20g / L, the concentration of sodium phytate is 0.5g / L, the temperature of the bath is 85°C, the formation voltage is 200V, and the current density is 70mA / cm 2 , the formation time is 7 minutes;
[0038] Step 4: In the second stage, the concentration of boric acid is 100g / L, the concentration of ammonium pentaborate is 4g / L, the concentration of sodium phytate is 0.3g / L, the temperature of the bath is 85°C, the formation voltage i...
Embodiment 2
[0049] Step 1: Take the 99.99% aluminum foil after electrolytic corrosion treatment and immerse it in pure water at 97°C for 20 minutes;
[0050] The second step: the pretreatment phosphoric acid concentration is 5ml / L, the sodium phytate concentration is 0.5g / L, the glucose concentration is 0.5g / L, the sodium bicarbonate concentration is 4g / L, the pH is 6.2, and the bath temperature is 60°C , the processing time is 3 minutes;
[0051] The third step: in the first stage, the concentration of boric acid is 100g / L, the concentration of ammonium pentaborate is 20g / L, the concentration of sodium phytate is 0.5g / L, the temperature of the bath is 85°C, the formation voltage is 200V, and the current density is 70mA / cm 2 , the formation time is 7 minutes;
[0052] Step 4: In the second stage, the concentration of boric acid is 100g / L, the concentration of ammonium pentaborate is 4g / L, the concentration of sodium phytate is 0.3g / L, the temperature of the bath is 85°C, the formation vo...
Embodiment 3
[0063] Step 1: Take the 99.99% aluminum foil after electrolytic corrosion treatment and immerse it in pure water at 97°C for 20 minutes;
[0064] The second step: the pretreatment phosphoric acid concentration is 2ml / L, the sodium phytate concentration is 0.25g / L, the glucose concentration is 0.25g / L, the sodium bicarbonate concentration is 3.2g / L, the pH is 5.8, and the bath temperature is 70 ℃, treatment time 2 minutes;
[0065] The third step: in the first stage, the concentration of boric acid is 100g / L, the concentration of ammonium pentaborate is 20g / L, the temperature of the bath solution is 85°C, the formation voltage is 200V, and the current density is 70mA / cm 2 , the formation time is 7 minutes;
[0066] Step 4: In the second stage, the concentration of boric acid is 100g / L, the concentration of ammonium pentaborate is 4g / L, the concentration of sodium phytate is 0.3g / L, the temperature of the bath is 85°C, the formation voltage is 400V, and the current density is 7...
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