Nano composite anti-corrosive coating
An anti-corrosion coating and nano-composite technology, applied in the field of nano-materials, can solve the problems of reducing the quality of the coating, easy to form agglomeration, high brittleness, etc., and achieve the effect of improving adhesion, enhancing binding force, and improving binding force.
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Embodiment 1
[0028] The preparation method of modified nano titanium nitride comprises the following steps:
[0029] Dissolve sodium lauryl sulfate in hot water at 70°C for stirring and dispersing, then add nano-titanium nitride for stirring and dispersing, ultrasonically treat for 1.5 hours, and then filter and dry to obtain modified nano-titanium nitride. The mass ratio of sodium lauryl sulfate to nano-titanium nitride is 7:1.
[0030] The effect of modification is measured by sedimentation experiment. Weigh 1-1.5g of the above-mentioned modified nano-titanium nitride sample and place it in a graduated cylinder with a ground mouth. First add a small amount of xylene to fully wet the nano-titanium nitride-graphene oxide. Finally, add xylene until 20mL is fully vibrated evenly, let it stand for different times under room temperature, record the mass of the sediment, and convert it into a sedimentation index; the sedimentation index=(mass of the sedimented part of the sample / total sample ma...
Embodiment 2
[0037] The preparation method of modified nano titanium nitride comprises the following steps:
[0038] Dissolve sodium lauryl sulfate in hot water at 80°C for stirring and dispersing, then add nano-titanium nitride for stirring and dispersing, ultrasonically treat for 0.5h, and then filter and dry to obtain modified nano-titanium nitride. The mass ratio of sodium lauryl sulfate to nano-titanium nitride is 5:1.
[0039] It can be seen from the test that the unmodified nano-titanium nitride-graphene oxide will completely settle down in xylene for about 3-5 hours, while the modified nano-titanium nitride will only settle in 1.2-1.8 hours after 24 hours in xylene. % precipitation, only about 2.6-3.2% precipitation after 48h. Therefore, the modified nano-titanium nitride has better dispersion performance and better modification effect.
[0040] The preparation method of modified silicone resin comprises the following steps:
[0041] 1) Calculated in parts by weight, weigh 50 pa...
Embodiment 3
[0045] A nanocomposite anticorrosion coating, calculated in parts by weight, comprising the following components:
[0046]50 parts of aqueous epoxy emulsions, 24 parts of modified silicone resins of embodiment 1, 9 parts of modified nano-titanium nitrides of embodiment 1, 7 parts of bentonite, 12 parts of sodium hexametaphosphate, 4 parts of alcohol ester twelve, 0.3 parts of sodium oleate, 0.9 parts of hydrogenated castor oil, 0.3 parts of emulsified methyl silicone oil and 25 parts of water.
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