Scutellaria baicalensis root extract as well as preparation method, application thereof and health care wine
A technology of scutellaria baicalensis extract and health wine, which is applied in the field of extraction of plant components, can solve problems such as difficulty in obtaining scutellaria baicalensis extract, affecting macroporous resin adsorption, loss of baicalin, etc., and achieves short cycle, low production cost, and low baicalin content. high effect
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[0029] see figure 1 As shown, the embodiment of the present invention provides a preparation method of Scutellaria baicalensis extract, which is to directly dilute the ethanol extract of Scutellaria baicalensis with water to an alcohol concentration of 10%-20%, and then apply macroporous resin for adsorption and separation and purification, thereby obtaining The extract of high-content baicalin specifically comprises the following steps:
[0030] (1) Dilution of the extract: take the ethanol extract of Scutellaria baicalensis, add water to dilute to an alcohol concentration of 10%-20%, and stir evenly to obtain a diluted extract.
[0031] In the present embodiment, the preparation method of Scutellaria baicalensis ethanol extract is:
[0032] Scutellaria baicalensis medicinal material and food-grade ethanol solution with a volume fraction of 50%-75%, the dosage ratio of scutellaria baicalensis medicinal material and ethanol solution is 1kg: 4-8L, heating and refluxing extract...
Embodiment 1
[0046] This embodiment provides a Scutellaria baicalensis extract, which is extracted by the following preparation method:
[0047] (1) Dilution of the extract: take 120L of Scutellaria baicalensis 50% ethanol extract (Scutellaria baicalensis medical material 10Kg), add 480L of pure water to dilute to an ethanol concentration of 10%, stir evenly to obtain a diluted extract.
[0048] (2) Resin adsorption: apply the diluted extract to LS-305 macroporous resin at a flow rate of 5BV / h, and then let it stand for 2 hours for adsorption after the sample is loaded.
[0049] (3) Resin elution: After the adsorption is completed, first add 8 times the amount of pure water for elution, then add 6 times the amount of 50% ethanol for elution, the elution rate is 3BV / h, and the eluent is obtained.
[0050] (4) Concentration and drying: the eluate was concentrated and dried to obtain 1031 g of Scutellaria baicalensis extract. After testing, the content of baicalin was 91.62%, and the yield w...
Embodiment 2
[0053] This embodiment provides a Scutellaria baicalensis extract, which is extracted by the following preparation method:
[0054] (1) Dilution of extract: take 120L of Scutellaria baicalensis 60% ethanol extract (Scutellaria baicalensis medicinal material 10Kg), add 360L of purified water to dilute to ethanol concentration of 15%, stir well to obtain diluted extract.
[0055] (2) Resin adsorption: apply the diluted extract to LS-306 macroporous resin at a flow rate of 7BV / h, and let it stand for adsorption for 1 hour after the sample loading is completed.
[0056] (3) Resin elution: After the adsorption is completed, first add 10 times the amount of pure water for elution, then add 5 times the amount of 60% ethanol for elution, the elution rate is 4BV / h, and the eluate is obtained.
[0057] (4) Concentration and drying: the eluate was concentrated and dried to obtain 1029 g of Scutellaria baicalensis extract. After testing, the content of baicalin was 91.87%, and the yield ...
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