Preparation method of self-slow-setting concrete
A kind of concrete, selected technology, applied in the field of preparation of self-retarding concrete
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[0021] The present invention also provides a kind of preparation method of self-retarding concrete, comprises the following steps:
[0022] (1) Evenly ball-mill bentonite and kaolin and calcinate at 300-450°C for 2-4 hours to obtain a mixed powder, then mill the mixed powder, diethylenetriaminepentamethylenephosphonic acid and gypsum in a ball mill, and then add water, and then microwave reaction at 80-95°C for 5-10 hours to obtain modified mineral powder;
[0023] (2) After uniformly mixing unsaturated glycerol, fatty alcohol polyoxyethylene ether, polyol, acid anhydride and polyamine in water, react at 80-120°C for 2-4 hours to obtain a slow-setting intermediate;
[0024] (3) After uniformly dispersing the retarder intermediate, fly ash, cement, fine sand, clay ceramsite, aluminum silicate fiber, modified mineral powder, and additives in water, continue stirring for 60-150s to obtain the self- retarded concrete.
[0025] In the present invention, first, bentonite, kaolin a...
Embodiment 1
[0028] A self-retarding concrete, made of the following raw materials in parts by weight: 30kg fly ash, 25kg cement, 22kg fine sand, 15kg clay ceramsite, 8kg bentonite, 12kg kaolin, 12kg gypsum, 2kg diethylenetriaminepenta Forkedphosphonic acid, 10kg aluminum silicate fiber, 8kg glycidyl methacrylate, 3kg fatty alcohol polyoxyethylene ether (purchased from Haidongqing Chemical Co., Ltd., AEO-9), 3kg polybutylene terephthalate , 2kg N-(2-aminoethyl)-1,3-propylenediamine, 4kg phthalic anhydride, 0.5kg polycarboxylate superplasticizer (model PASP-Ca, purchased from Shandong Yuanlian Chemical Co., Ltd.) , 1kg sodium dodecylbenzenesulfonate, 0.5kg calcium stearate, 0.5kg hydroxyethyl methyl reinforced cellulose ether, 0.5kg sodium aluminate.
[0029] The preparation steps of described self-retarding concrete are as follows:
[0030] (1) After uniform ball milling of bentonite and kaolin, calcining at 350°C for 3 hours to obtain a mixed powder, then ball milling the mixed powder, d...
Embodiment 2
[0034]A self-retarding concrete, made of the following raw materials in parts by weight: 36kg fly ash, 30kg cement, 16kg fine sand, 18kg clay ceramsite, 6kg bentonite, 8kg kaolin, 6kg gypsum, 2kg diethylene triamine pentamethyl Forkedphosphonic acid, 12kg aluminum silicate fiber, 5kg 2-glycidyl methacrylate, 5kg fatty alcohol polyoxyethylene ether (purchased from Costin Chemical Co., Ltd., AEO-9), 2kg polyoxypropylene glycol, 3kg Diethylenetriamine, 6kg maleic acid, 1kg polycarboxylate water reducer (model PASP-Ca, purchased from Shandong Yuanlian Chemical Co., Ltd.), 1kg sodium dodecylbenzenesulfonate, 1kg stearic acid Calcium, 1kg hydroxyethyl methyl reinforced cellulose ether, 1kg sodium aluminate.
[0035] The preparation steps of described self-retarding concrete are as follows:
[0036] (1) After uniform ball milling of bentonite and kaolin, calcining at 450°C for 2 hours to obtain a mixed powder, then ball milling the mixed powder, diethylenetriaminepentamethylenephosp...
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