Method for detecting Yinqiao detoxification mixture

Abstract

The invention relates to a method for detecting a Yinqiao detoxification mixture. The method comprises trait, component identification and inspection items, wherein the component identification comprises thin layer chromatography identification of flos genkwa, thin layer chromatography identification of flos lonicerae, thin layer chromatography identification of herba menthae, thin layer chromatography identification of fructus forsythiae and thin layer chromatography identification of fructus arctii and licorice root. The method is carried out aiming at the problem that a conventional detection method cannot conduct corresponding monitoring on effective components and cannot detect the mixing of the fake flos genkwa, the scientific, reasonable and feasible component identification methodis formulated, a low-toxic and non-toxic reagent is adopted to replace trichloromethane, environmental pollution is reduced, damage to the health of inspectors is reduced, clinical effects of drugs are ensured, and the fake flos genkwa in the flos lonicerae can also be effectively detected to avoid toxic and harmful components which endanger the health of patients.

Description

Technical field [0001] The invention relates to a method for detecting a mixture of traditional Chinese medicine, in particular to a method for detecting a mixture of Yinqiaojiedu. Background technique [0002] Yinqiao Jiedu Mixture is a variety included in the 14th volume of Chinese Medicine Prescription Preparations of the Ministry of Health Drug Standards. The standard number is WS3-B-2783-97. The prescription is honeysuckle, forsythia, peppermint, nepeta, light tempeh, Burdock seed, Platycodon grandiflorum, pale bamboo leaves, licorice, is a mixture of pure Chinese medicine, which has the effects of pungent cooling and relieving surface, clearing heat and detoxification. It is currently clinically used for wind-heat and cold, fever, headache, cough, dry mouth, and sore throat. [0003] The testing standards for Yinqiao Jiedu Mixture were formulated in the 1990s and have historical limitations: on the one hand, chloroform, namely chloroform, and n-hexane are used in the testing ...

AI Technical Summary

Problems solved by technology

[0003] The detection standard of Yinqiao Jiedu Mixture was formulated in the 1990s, and has historical limitations: on the one hand, chloroform, that is, trichloromethane, and n-hexane are used in the test method, which are highly toxic, not only Pollution of the environment will also damage the health of inspectors; on the other hand, honeysuckle is the most used in prescriptions. Since honeysuckle is a commonly used medicine and belongs to the same source of medicine and food, the amount of use is relatively large, but the output of honeysuckle is very limited. , so its substitutes and counterfeit products are also used intentionally or unintentionally. One of the counterfeit products that is easily mixed in is genkwa. In places where people use it to poison rats and fish, it is harmful to people's health if it is strayed into medicine

At the same time, there is no effective detection method for honeysuckle, the most expensive medicinal material used in prescriptions, which leads to the inability to monitor the quality of medicines well.