Motor vehicle antifreeze fluid and preparation method thereof
A technology of automobile antifreeze and antifreeze, which is applied in the direction of chemical instruments and methods, heat exchange materials, etc., can solve the problems of engine temperature rise, coolant thermal conductivity reduction, easy scale formation, etc., to delay the formation time and heat conduction Reduced resistance, good anti-freeze sticking performance
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[0022] A preparation method for automobile antifreeze, comprising the steps of:
[0023] In parts by mass, take 55~58 parts of ethylene glycol, 40~45 parts of water, 0.3~0.5 parts of glycine, 0.5~0.7 parts of triethanolamine, 3~5 parts of red dye, 12~15 parts of antifreeze additive a , 8~12 parts of antifreeze additive b and 12~15 parts of antifreeze additive c are mixed to obtain automobile antifreeze.
Embodiment 1
[0025] Waste oil: from the university cafeteria.
[0026] Water-based acrylic emulsion: purchased from Foshan Tongde Chemical Company; nano-silica: purchased from German BYK Chemical Company.
[0027]Antioxidant: Take the fruit of myrobalan fruit and dry it, crush it through an 80-mesh sieve, collect the sieved particles, add acetone solution with a mass fraction of 70% at a mass ratio of 1:4, ultrasonically extract at 25°C for 50 minutes, repeat twice, and combine the extracts. Concentrate under reduced pressure, take the reduced-pressure concentrate and add ethyl acetate for extraction at a mass ratio of 1:3, take the extract and concentrate under reduced pressure to obtain an antioxidant.
[0028] Antifreeze additive a: Take gutter oil and add p-hydroxydiphenylamine at a mass ratio of 45:1, stir and mix at 35°C for 20 minutes, take the mixture and add activated carbon and antioxidants at a mass ratio of 10:4:3, raise the temperature to 95°C and keep for 1 hour, Let it stan...
Embodiment 2
[0034] Waste oil: from the university cafeteria.
[0035] Water-based acrylic emulsion: purchased from Foshan Tongde Chemical Company; nano-silica: purchased from German BYK Chemical Company.
[0036] Antioxidant: take the fruit of myrobalan fruit and dry it, crush it through an 80-mesh sieve, collect the sieved particles, add acetone solution with a mass fraction of 70% according to the mass ratio of 1:4, ultrasonically extract at 30°C for 60 minutes, repeat 3 times, and combine the extracts. Concentrate under reduced pressure, take the reduced-pressure concentrate and add ethyl acetate for extraction at a mass ratio of 1:3, take the extract and concentrate under reduced pressure to obtain an antioxidant.
[0037] Antifreeze additive a: take gutter oil and add p-hydroxydiphenylamine at a mass ratio of 45:1, stir and mix at 40°C for 30 minutes, take the mixture and add activated carbon and antioxidants at a mass ratio of 10:4:3, raise the temperature to 100°C and keep for 2 ho...
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