Nano-silica particle packed bed super thermal insulation material and preparation method thereof
A technology of nano-silica and particle accumulation, applied in ceramic products, other household appliances, applications, etc., can solve the problems of insignificant improvement of mechanical properties of thermal insulation materials and increase of material costs, achieve strong mechanical properties and reduce air convection Thermal, environmentally friendly effect
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Embodiment 1
[0021] A method for preparing a nano-silica particle packed bed super heat-insulating material, comprising the following steps:
[0022] (1) Under room temperature conditions, the nano-silica particles A with a particle diameter of 10nm and the nano-silica particles B with a particle diameter of 50nm are put into a ball mill with a mass ratio of 5:5, and the ball mill is first Ball milling at a speed of 200r / min for 60min, then ball milling at a speed of 100r / min for 60min, and mix uniformly to obtain nano-silica mixed particles A;
[0023] (2) Transfer nano-silica mixed particles A to an ultrasonic disperser, then add an infrared shielding agent to the ultrasonic disperser for ultrasonic dispersion for 50 minutes to obtain nano-silica mixed particles B, and the infrared shielding agent and nano-dioxide The mass ratio of silicon mixed particles A is 1:10; the infrared shielding agent is a mixture of potassium titanate whiskers and SiC nanoparticles, and the mass ratio of potas...
Embodiment 2
[0027] A method for preparing a nano-silica particle packed bed super heat-insulating material, comprising the following steps:
[0028] (1) Under room temperature conditions, the nano-silica particles A with a particle diameter of 25nm and the nano-silica particles B with a particle diameter of 75nm are put into a ball mill with a mass ratio of 7:3, and the ball mill is first Ball milling at a speed of 200r / min for 60min, then ball milling at a speed of 100r / min for 60min, and mix uniformly to obtain nano-silica mixed particles A;
[0029] (2) Transfer the nano-silica mixed particles A to an ultrasonic disperser, then add an infrared shielding agent to the ultrasonic disperser for ultrasonic dispersion for 60 minutes to obtain a nano-silica mixed particle B, and the infrared shielding agent and nano-dioxide The mass ratio of silicon mixed particles A is 1:10; the infrared shielding agent is a mixture of potassium titanate whiskers and SiC nanoparticles, and the mass ratio of ...
Embodiment 3
[0033]A method for preparing a nano-silica particle packed bed super heat-insulating material, comprising the following steps:
[0034] (1) Under room temperature conditions, the nano-silica particles A with a particle diameter of 40nm and the nano-silica particles B with a particle diameter of 100nm are put into a ball mill with a mass ratio of 8:2, and the ball mill is first Ball milling at a speed of 200r / min for 60min, then ball milling at a speed of 100r / min for 60min, and mix uniformly to obtain nano-silica mixed particles A;
[0035] (2) Transfer the nano-silica mixed particles A to an ultrasonic disperser, then add an infrared shielding agent to the ultrasonic disperser for ultrasonic dispersion for 70 minutes to obtain a nano-silica mixed particle B, and the infrared shielding agent and nano-dioxide The mass ratio of silicon mixed particles A is 1:8; the infrared shielding agent is a mixture of potassium titanate whiskers and SiC nanoparticles, and the mass ratio of p...
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