Medical self-adhesive elastic bandage preparation method
A self-adhesive elastic bandage, medical technology, applied in bandages, medical science, absorbent pads and other directions, can solve the problems of human skin allergy, not easy to tear, feel greasy, etc., achieve excellent air permeability, strong acid and alkali resistance, reduce stimulatory effect
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Embodiment 1
[0016] A preparation method of medical self-adhesive elastic bandage, comprising the following steps:
[0017] (1) In parts by weight, mix 32 parts of methacrylic anhydride, 18 parts of methyl methacrylate, 10 parts of methyl acrylate, 24 parts of deionized water, and 3 parts of dodecylamine, and heat to 75°C, Stir continuously for 60min to prepare mixed emulsion;
[0018] (2) Slowly add the modifier to the mixed emulsion prepared in step (1), raise the temperature of the mixed solution to 86°C, keep stirring for 300 minutes, cool to room temperature, and filter with a 150-mesh sieve. A binder is prepared, wherein the modifying agent is made of the following components by weight: 16 parts of trifluoroethyl acrylate, 35 parts of methyl tributylketoximosilane, and 3 parts of potassium persulfate;
[0019] (3) After adding a stabilizer to the adhesive prepared in step (2), stir evenly, and then paint the prepared adhesive on both sides of the elastic bandage to obtain a medical ...
Embodiment 2
[0025] A preparation method of medical self-adhesive elastic bandage, comprising the following steps:
[0026] (1) In parts by weight, mix 34 parts of methacrylic anhydride, 20 parts of methyl methacrylate, 14 parts of methyl acrylate, 26 parts of deionized water, and 5 parts of dodecylamine, and heat it to 78°C. Stir continuously for 65min to obtain a mixed emulsion;
[0027] (2) Slowly add the modifier to the mixed emulsion prepared in step (1), raise the temperature of the mixed solution to 88°C, keep stirring for 330 minutes, cool to room temperature, and filter with a 150-mesh sieve. A binder is prepared, wherein the modifying agent is made of the following components by weight: 20 parts of trifluoroethyl acrylate, 38 parts of methyl tributylketoxime silane, and 5 parts of potassium persulfate;
[0028] (3) After adding a stabilizer to the adhesive prepared in step (2), stir evenly, and then paint the prepared adhesive on both sides of the elastic bandage to obtain a med...
Embodiment 3
[0034] A preparation method of medical self-adhesive elastic bandage, comprising the following steps:
[0035] (1) In parts by weight, after mixing 36 parts of methacrylic anhydride, 22 parts of methyl methacrylate, 16 parts of methyl acrylate, 30 parts of deionized water and 6 parts of dodecylamine, heated to 80°C, Stir continuously for 70min to prepare mixed emulsion;
[0036] (2) Slowly add the modifier to the mixed emulsion prepared in step (1), raise the temperature of the mixed solution to 90°C, keep stirring for 350 minutes, cool to room temperature, and filter with a 150-mesh sieve. A binder is prepared, wherein the modifying agent is made of the following components by weight: 22 parts of trifluoroethyl acrylate, 40 parts of methyl tributylketoximosilane, and 6 parts of potassium persulfate;
[0037] (3) After adding a stabilizer to the adhesive prepared in step (2), stir evenly, and then paint the prepared adhesive on both sides of the elastic bandage to obtain a me...
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