Composite material for water ecological restoration, and preparation method and application thereof
A composite material, water ecology technology, applied in chemical instruments and methods, water pollutants, water/sewage treatment, etc., can solve problems such as poor restoration effect, deterioration of water environment, single function, etc. Simple preparation process
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Embodiment 1
[0023] In an embodiment of the present invention, a composite material for water ecological restoration includes the following raw materials: 30 kg of bran, 8 kg of itaconic acid, 3 kg of diethylenetriamine, 26 kg of tea bran, 1 kg of dichloroethane, and potassium fulvic acid 11kg.
[0024] Mix dichloroethane with 3-4 times the mass of ethanol, crush the tea bran, pass through a 100-mesh sieve, then add the dichloroethane solution, then raise the temperature to 70°C and at this temperature, stir at a speed of 350r / min Heat and stir for 30 minutes, then ultrasonically treat for 10 minutes, the ultrasonic power is 600W, add deionized water twice the amount of tea bran, mix and stir for 10 minutes at a stirring speed of 350r / min, filter the filtrate of the water layer, and concentrate to 10% of its volume , to prepare tea bran treatment. Mix itaconic acid with 8 times its mass of ethanol to prepare itaconic acid solution; crush the bran and pass through a 100-mesh sieve, then mi...
Embodiment 2
[0026] In an embodiment of the present invention, a composite material for water ecological restoration includes the following raw materials: 40 kg of bran, 16 kg of itaconic acid, 7 kg of diethylenetriamine, 34 kg of tea bran, 5 kg of dichloroethane, and potassium fulvic acid 19kg.
[0027] Mix dichloroethane with 4 times its mass of ethanol, crush the tea bran, pass through a 150-mesh sieve, then add the dichloroethane solution, then raise the temperature to 75°C and heat and stir at a stirring speed of 400r / min at this temperature 40min, then ultrasonic treatment for 20min, the ultrasonic power is 600W, add deionized water with 3 times the amount of tea bran, after mixing and stirring for 15min at a stirring speed of 400r / min, filter the water layer filtrate, and concentrate to 15% of its volume to prepare Get tea bran treatment. Mix itaconic acid with 10 times its mass of ethanol to prepare itaconic acid solution; crush the bran and pass through a 150-mesh sieve, then mix...
Embodiment 3
[0029] In an embodiment of the present invention, a composite material for water ecological restoration includes the following raw materials: bran 32kg, itaconic acid 10kg, diethylenetriamine 4kg, tea bran 28kg, dichloroethane 2kg, potassium fulvic acid 13kg.
[0030] Mix dichloroethane with 3.5 times its mass of ethanol, crush the tea bran, pass through a 150-mesh sieve, then add the dichloroethane solution, then raise the temperature to 72°C and heat and stir at a stirring speed of 400r / min at this temperature 40min, then ultrasonic treatment for 20min, the ultrasonic power is 600W, add deionized water with 3 times the amount of tea bran, after mixing and stirring for 15min at a stirring speed of 400r / min, filter the water layer filtrate, and concentrate to 15% of its volume to prepare Get tea bran treatment. Mix itaconic acid with 9 times its mass of ethanol to obtain an itaconic acid solution; crush the bran and pass through a 150-mesh sieve, then mix and stir with itacon...
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