Method for preparing reduced leather based on combination of collagen fiber grey fabric, flocking process and solvent-free resin process
A technology of collagen fiber and solvent-free resin, which is applied in the direction of textiles and papermaking, can solve the problems of leather preparation in the finishing process, achieve rich hand feeling, improve flatness, and improve the effect of surface smoothness
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Embodiment 1
[0033] Embodiment 1 Adopt the following steps to realize the present invention:
[0034] 1. Collagen fiber preparation: adopt the preparation method of collagen fiber for direct spinning in Example 2 of patent ZL201510228478.4, use wet blue leather as raw material and go through shearing, ultrasonic pretreatment, drum treatment, liquid fiber disintegration, and fiber The steps of drying, opening and removing impurities, carding, and fiber surface treatment are used to obtain collagen fibers, and then the collagen fibers are spun into yarn by spinning technology, and the base cloth is woven to obtain collagen fiber gray cloth; the specific steps are as follows:
[0035] (1) Cutting: use wet blue leather as raw material, and cut it into the size required by production or equipment with a leather shearing machine;
[0036] (2) Ultrasonic pretreatment: Prepare a polar solvent pretreatment solution rich in hydroxyl groups, adjust the pH to 7, raise the temperature to 45°C, complete...
Embodiment 2
[0054] Embodiment 2 The following steps are adopted to realize the preparation of reduced skin of the present invention:
[0055] 1. Preparation of collagen fiber gray cloth: adopt the preparation method of collagen fiber for direct spinning described in Example 4 of patent ZL201510228478.4, use wet blue leather as raw material and go through shearing, ultrasonic pretreatment, drum treatment, liquid The specific steps for producing collagen fibers are as follows:
[0056] (1) Cutting: use wet blue leather as raw material, and cut it into the size required by production or equipment with a leather shearing machine;
[0057] (2) Ultrasonic pretreatment: Prepare the pretreatment solution, adjust the pH to 7.5, raise the temperature to 40°C, completely immerse the cut wet blue leather in the pretreatment solution for 20 hours, then raise the temperature of the pretreatment solution to 60°C, and adjust the pH 7.5, then soak for 1 hour, and perform ultrasonic low-frequency short-te...
Embodiment 3
[0074] Embodiment 3 Use the following steps to realize the preparation of the reduced skin of the present invention:
[0075] 1. Preparation of collagen fiber gray cloth: adopt the preparation method of collagen fiber for direct spinning described in Example 3 of patent ZL201510228478.4, use wet blue leather as raw material through shearing, ultrasonic pretreatment, drum treatment, liquid Collagen fibers are obtained through the steps of fiber disintegration, fiber drying, opening and impurity removal, carding, and fiber surface treatment. The specific steps are as follows:
[0076] (1) Cutting: use wet blue leather as raw material, cut it into the size required by production or equipment with a leather shearing machine, immerse the wet blue leather raw material in a water pool for 2 to 5 minutes, and dry until the moisture content is 60 to 80%;
[0077] (2) Ultrasonic pretreatment: Prepare the pretreatment solution, adjust the pH to 7, raise the temperature to 50°C, completel...
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